N-(3-(4-oxido-4-morpholino)propyl)-(2S,4S,5S)-5-((tert-butyloxycarbonyl)amino)-6-cyclohexyl-4-hydroxy-2-isopropylhexanamide

Base Information

Chemical Name:N-(3-(4-oxido-4-morpholino)propyl)-(2S,4S,5S)-5-((tert-butyloxycarbonyl)amino)-6-cyclohexyl-4-hydroxy-2-isopropylhexanamide
CAS No.:142687-65-8
Molecular Formula:C₂₇H₅₁N₃O₆
Molecular Weight:513.718
Hs Code.:

Synonyms:N-(3-(4-oxido-4-morpholino)propyl)-(2S,4S,5S)-5-((tert-butyloxycarbonyl)amino)-6-cyclohexyl-4-hydroxy-2-isopropylhexanamide

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Chemical Property of N-(3-(4-oxido-4-morpholino)propyl)-(2S,4S,5S)-5-((tert-butyloxycarbonyl)amino)-6-cyclohexyl-4-hydroxy-2-isopropylhexanamide

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Technology Process of N-(3-(4-oxido-4-morpholino)propyl)-(2S,4S,5S)-5-((tert-butyloxycarbonyl)amino)-6-cyclohexyl-4-hydroxy-2-isopropylhexanamide

There total 3 articles about N-(3-(4-oxido-4-morpholino)propyl)-(2S,4S,5S)-5-((tert-butyloxycarbonyl)amino)-6-cyclohexyl-4-hydroxy-2-isopropylhexanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 142688-84-4
N-(3-(4-morpholino)propyl)-(2S,4S,5S)-5-((tert-butyloxycarbonyl)amino)-6-cyclohexyl-4-hydroxy-2-isopropylhexanamide

: 142687-65-8
N-(3-(4-oxido-4-morpholino)propyl)-(2S,4S,5S)-5-((tert-butyloxycarbonyl)amino)-6-cyclohexyl-4-hydroxy-2-isopropylhexanamide

Guidance literature:: With dihydrogen peroxide; In methanol; at 50 ℃; for 48h;
DOI:10.1021/jm00045a003

Reference yield:

: 123-00-2
4-(3-Aminopropyl)morpholine

: 142687-65-8
N-(3-(4-oxido-4-morpholino)propyl)-(2S,4S,5S)-5-((tert-butyloxycarbonyl)amino)-6-cyclohexyl-4-hydroxy-2-isopropylhexanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / 96 h / 60 °C

2: 92 percent / 30percent aq. H₂O₂ / methanol / 48 h / 50 °C

With dihydrogen peroxide; In methanol;
DOI:10.1021/jm00045a003

Reference yield:

: 124032-36-6
(3S,5S)-5-[(1S)-1-(t-butoxycarbonyl)amino-2-cyclohexylethyl]-3-isopropyldihydrofuran-2(3H)-one

: 142687-65-8
N-(3-(4-oxido-4-morpholino)propyl)-(2S,4S,5S)-5-((tert-butyloxycarbonyl)amino)-6-cyclohexyl-4-hydroxy-2-isopropylhexanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / 96 h / 60 °C

2: 92 percent / 30percent aq. H₂O₂ / methanol / 48 h / 50 °C

With dihydrogen peroxide; In methanol;
DOI:10.1021/jm00045a003