tert-butyl 4-(((tert-butyloxycarbonyl)(4-formyl-2-methoxyphenyl)amino)methyl)phenylcarbamate

Base Information

Chemical Name:tert-butyl 4-(((tert-butyloxycarbonyl)(4-formyl-2-methoxyphenyl)amino)methyl)phenylcarbamate
CAS No.:1612184-54-9
Molecular Formula:C₂₅H₃₂N₂O₆
Molecular Weight:456.539
Hs Code.:

Synonyms:tert-butyl 4-(((tert-butyloxycarbonyl)(4-formyl-2-methoxyphenyl)amino)methyl)phenylcarbamate

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Chemical Property of tert-butyl 4-(((tert-butyloxycarbonyl)(4-formyl-2-methoxyphenyl)amino)methyl)phenylcarbamate

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Technology Process of tert-butyl 4-(((tert-butyloxycarbonyl)(4-formyl-2-methoxyphenyl)amino)methyl)phenylcarbamate

There total 7 articles about tert-butyl 4-(((tert-butyloxycarbonyl)(4-formyl-2-methoxyphenyl)amino)methyl)phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.7%

: 1612184-57-2
tert-butyl 4-(((tert-butyloxycarbonyl)(4-(hydroxymethyl)-2-methoxyphenyl)amino)methyl)phenylcarbamate

: 1612184-54-9
tert-butyl 4-(((tert-butyloxycarbonyl)(4-formyl-2-methoxyphenyl)amino)methyl)phenylcarbamate

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 1.5h; Darkness;

Reference yield:

: 882430-21-9
tert-butyl(3-methoxy-4-nitrobenzyloxy)dimethylsilane

: 1612184-54-9
tert-butyl 4-(((tert-butyloxycarbonyl)(4-formyl-2-methoxyphenyl)amino)methyl)phenylcarbamate

Guidance literature:: Multi-step reaction with 6 steps

1: platinum(IV) oxide; hydrogen / ethyl acetate / 4 h / 20 °C

2: magnesium sulfate; sodium sulfate / dichloromethane / 72 h / 20 °C / Inert atmosphere

3: sodium tetrahydroborate; ethanol / tetrahydrofuran; ethanol / 0.5 h / 20 °C / Inert atmosphere

4: sodium hydrogencarbonate / tetrahydrofuran; water / 72 h / 20 °C

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 12 h / 20 °C

6: pyridinium chlorochromate / dichloromethane / 1.5 h / 20 °C / Darkness

With platinum(IV) oxide; sodium tetrahydroborate; ethanol; tetrabutyl ammonium fluoride; hydrogen; sodium hydrogencarbonate; magnesium sulfate; sodium sulfate; pyridinium chlorochromate; In tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate;

Reference yield:

: 882430-23-1
4-((tert-butyldimethylsilyloxy)methyl)-2-methoxyaniline

: 1612184-54-9
tert-butyl 4-(((tert-butyloxycarbonyl)(4-formyl-2-methoxyphenyl)amino)methyl)phenylcarbamate

Guidance literature:: Multi-step reaction with 5 steps

1: magnesium sulfate; sodium sulfate / dichloromethane / 72 h / 20 °C / Inert atmosphere

2: sodium tetrahydroborate; ethanol / tetrahydrofuran; ethanol / 0.5 h / 20 °C / Inert atmosphere

3: sodium hydrogencarbonate / tetrahydrofuran; water / 72 h / 20 °C

4: tetrabutyl ammonium fluoride / tetrahydrofuran / 12 h / 20 °C

5: pyridinium chlorochromate / dichloromethane / 1.5 h / 20 °C / Darkness

With sodium tetrahydroborate; ethanol; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; magnesium sulfate; sodium sulfate; pyridinium chlorochromate; In tetrahydrofuran; ethanol; dichloromethane; water;