tert-butyl 4-((4-((tert-butyldimethylsilyloxy)methyl)-2-methoxyphenylamino)methyl)phenylcarbamate

Base Information

Chemical Name:tert-butyl 4-((4-((tert-butyldimethylsilyloxy)methyl)-2-methoxyphenylamino)methyl)phenylcarbamate
CAS No.:1612184-55-0
Molecular Formula:C₂₆H₄₀N₂O₄Si
Molecular Weight:472.7
Hs Code.:

Synonyms:tert-butyl 4-((4-((tert-butyldimethylsilyloxy)methyl)-2-methoxyphenylamino)methyl)phenylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl 4-((4-((tert-butyldimethylsilyloxy)methyl)-2-methoxyphenylamino)methyl)phenylcarbamate

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Technology Process of tert-butyl 4-((4-((tert-butyldimethylsilyloxy)methyl)-2-methoxyphenylamino)methyl)phenylcarbamate

There total 5 articles about tert-butyl 4-((4-((tert-butyldimethylsilyloxy)methyl)-2-methoxyphenylamino)methyl)phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₆H₃₈N₂O₄Si

: 1612184-55-0
tert-butyl 4-((4-((tert-butyldimethylsilyloxy)methyl)-2-methoxyphenylamino)methyl)phenylcarbamate

Guidance literature:: With sodium tetrahydroborate; ethanol; In tetrahydrofuran; ethanol; at 20 ℃; for 0.5h; Inert atmosphere;

Reference yield:

: 882430-21-9
tert-butyl(3-methoxy-4-nitrobenzyloxy)dimethylsilane

: 1612184-55-0
tert-butyl 4-((4-((tert-butyldimethylsilyloxy)methyl)-2-methoxyphenylamino)methyl)phenylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: platinum(IV) oxide; hydrogen / ethyl acetate / 4 h / 20 °C

2: magnesium sulfate; sodium sulfate / dichloromethane / 72 h / 20 °C / Inert atmosphere

3: sodium tetrahydroborate; ethanol / tetrahydrofuran; ethanol / 0.5 h / 20 °C / Inert atmosphere

With platinum(IV) oxide; sodium tetrahydroborate; ethanol; hydrogen; magnesium sulfate; sodium sulfate; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate;

Reference yield:

: 80866-88-2
(3-methoxy-4-nitrophenyl)methanol

: 1612184-55-0
tert-butyl 4-((4-((tert-butyldimethylsilyloxy)methyl)-2-methoxyphenylamino)methyl)phenylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1: 1H-imidazole / dichloromethane / 1 h / 0 °C

2: platinum(IV) oxide; hydrogen / ethyl acetate / 4 h / 20 °C

3: magnesium sulfate; sodium sulfate / dichloromethane / 72 h / 20 °C / Inert atmosphere

4: sodium tetrahydroborate; ethanol / tetrahydrofuran; ethanol / 0.5 h / 20 °C / Inert atmosphere

With 1H-imidazole; platinum(IV) oxide; sodium tetrahydroborate; ethanol; hydrogen; magnesium sulfate; sodium sulfate; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate;