4-(4-aza-tricyclo[5.2.1.0(2,6)]dec-8-en-4-yl)-benzoic acid 4-hexadecyloxy-3,5-diiodobenzyl ester

Base Information

Chemical Name:4-(4-aza-tricyclo[5.2.1.0(2,6)]dec-8-en-4-yl)-benzoic acid 4-hexadecyloxy-3,5-diiodobenzyl ester
CAS No.:1314653-36-5
Molecular Formula:C₃₉H₅₃I₂NO₃
Molecular Weight:837.664
Hs Code.:

Synonyms:4-(4-aza-tricyclo[5.2.1.0(2,6)]dec-8-en-4-yl)-benzoic acid 4-hexadecyloxy-3,5-diiodobenzyl ester

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Chemical Property of 4-(4-aza-tricyclo[5.2.1.0(2,6)]dec-8-en-4-yl)-benzoic acid 4-hexadecyloxy-3,5-diiodobenzyl ester

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Technology Process of 4-(4-aza-tricyclo[5.2.1.0(2,6)]dec-8-en-4-yl)-benzoic acid 4-hexadecyloxy-3,5-diiodobenzyl ester

There total 5 articles about 4-(4-aza-tricyclo[5.2.1.0(2,6)]dec-8-en-4-yl)-benzoic acid 4-hexadecyloxy-3,5-diiodobenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 946091-06-1
4-(4-aza-tricyclo[5.2.1.0^2,6]dec-8-en-4-yl)benzoic acid chloride

: 1314653-35-4
4-hexadecyloxy-3,5-diiodobenzyl alcohol

: 1314653-36-5
4-(4-aza-tricyclo[5.2.1.0(2,6)]dec-8-en-4-yl)-benzoic acid 4-hexadecyloxy-3,5-diiodobenzyl ester

Guidance literature:: With dmap; In dichloromethane; at 20 ℃;
DOI:10.1002/asia.201000877

Reference yield:

: 877154-50-2
4-(4-aza-tricyclo[5.2.1.0^2,6]dec-8-en-4-yl)benzoic acid

: 1314653-36-5
4-(4-aza-tricyclo[5.2.1.0(2,6)]dec-8-en-4-yl)-benzoic acid 4-hexadecyloxy-3,5-diiodobenzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane

2: dmap / dichloromethane / 20 °C

With dmap; oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1002/asia.201000877

Reference yield:

: 1314653-33-2
4-(hexadecyloxy)-3,5-diiodobenzaldehyde

: 1314653-36-5
4-(4-aza-tricyclo[5.2.1.0(2,6)]dec-8-en-4-yl)-benzoic acid 4-hexadecyloxy-3,5-diiodobenzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium tetrahydroborate / methanol; dichloromethane / 3 h / 0 - 20 °C

1.2: Saturated solution

2.1: dmap / dichloromethane / 20 °C

With dmap; sodium tetrahydroborate; In methanol; dichloromethane;
DOI:10.1002/asia.201000877