C₂₆H₂₈FN₃O₅

Base Information

Chemical Name:C₂₆H₂₈FN₃O₅
CAS No.:1186047-02-8
Molecular Formula:C₂₆H₂₈FN₃O₅
Molecular Weight:481.524
Hs Code.:

C<sub>26</sub>H<sub>28</sub>FN<sub>3</sub>O<sub>5</sub>

Synonyms:C₂₆H₂₈FN₃O₅

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Chemical Property of C₂₆H₂₈FN₃O₅

Chemical Property:

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Technology Process of C₂₆H₂₈FN₃O₅

There total 9 articles about C₂₆H₂₈FN₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1186047-01-7
C₂₃H₂₄FN₃O₄

: 78-95-5
chloroacetone

: 1186047-02-8
C₂₆H₂₈FN₃O₅

Guidance literature:: C₂₃H₂₄FN₃O₄; chloroacetone; With potassium carbonate; In acetone; at 20 ℃;

With caesium carbonate; In acetone; Reflux;

Reference yield:

: 403-40-7
1-(4-fluorophenyl)ethylamine

: 1186047-02-8
C₂₆H₂₈FN₃O₅

Guidance literature:: Multi-step reaction with 9 steps

1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 60 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 70 °C

4.1: sodium tetrahydroborate; calcium chloride / methanol / 0 - 20 °C

5.1: copper(l) iodide; dicyclohexyl-carbodiimide / toluene / 1 h / 105 °C

6.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 0 °C

6.2: 0 °C

7.1: tin(ll) chloride / ethanol / 2 h / Reflux

8.1: acetic anhydride / Cooling

8.2: 1 h

9.1: potassium carbonate / acetone / 20 °C

9.2: Reflux

With sodium tetrahydroborate; N-Bromosuccinimide; copper(l) iodide; acetic anhydride; sodium hydride; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; dicyclohexyl-carbodiimide; calcium chloride; tin(ll) chloride; In tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide; acetone; toluene; mineral oil;

Reference yield:

: 1119-46-6
5-chloro-valeric acid

: 1186047-02-8
C₂₆H₂₈FN₃O₅

Guidance literature:: Multi-step reaction with 9 steps

1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 60 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 70 °C

4.1: sodium tetrahydroborate; calcium chloride / methanol / 0 - 20 °C

5.1: copper(l) iodide; dicyclohexyl-carbodiimide / toluene / 1 h / 105 °C

6.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 0 °C

6.2: 0 °C

7.1: tin(ll) chloride / ethanol / 2 h / Reflux

8.1: acetic anhydride / Cooling

8.2: 1 h

9.1: potassium carbonate / acetone / 20 °C

9.2: Reflux

With sodium tetrahydroborate; N-Bromosuccinimide; copper(l) iodide; acetic anhydride; sodium hydride; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; dicyclohexyl-carbodiimide; calcium chloride; tin(ll) chloride; In tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide; acetone; toluene; mineral oil;