2,3,4,5-tetramethoxyphenylboronic acid

Base Information

Chemical Name:2,3,4,5-tetramethoxyphenylboronic acid
CAS No.:857674-57-8
Molecular Formula:C₁₀H₁₅BO₆
Molecular Weight:242.036
Hs Code.:

Synonyms:2,3,4,5-tetramethoxyphenylboronic acid

Suppliers and Price of 2,3,4,5-tetramethoxyphenylboronic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2,3,4,5-tetramethoxyphenylboronic acid

Chemical Property:

Purity/Quality:: 95%-98% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

MSDS Files:

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Technology Process of 2,3,4,5-tetramethoxyphenylboronic acid

There total 3 articles about 2,3,4,5-tetramethoxyphenylboronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 21450-56-6
1,2,3,4-tetramethoxybenzene

: 857674-57-8
2,3,4,5-tetramethoxyphenylboronic acid

Guidance literature:: With n-butyllithium; Trimethyl borate; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1021/np5002048

Reference yield:

: 121-43-7,63156-11-6
Trimethyl borate

: 21450-56-6
1,2,3,4-tetramethoxybenzene

: 857674-57-8
2,3,4,5-tetramethoxyphenylboronic acid

Guidance literature:: 1,2,3,4-tetramethoxybenzene; With n-butyllithium; In tetrahydrofuran;

Trimethyl borate; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/j.bmcl.2010.07.111

Reference yield:

: 19676-64-3
2,3,4-trimethoxyphenol

: 857674-57-8
2,3,4,5-tetramethoxyphenylboronic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: 89 percent / K₂CO₃ / acetone / 6 h / Heating

2.1: n-BuLi / tetrahydrofuran; hexane / 1.5 h / 20 °C

2.2: B(OMe)3 / tetrahydrofuran; hexane / 3 h / -78 - 20 °C

2.3: aq. HCl / tetrahydrofuran; hexane / 2 h / 0 - 20 °C

With n-butyllithium; potassium carbonate; In tetrahydrofuran; hexane; acetone;
DOI:10.1021/ol0507569