5,9-di(phenylsulfonyl)-1-phenylthio-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraene

Base Information

Chemical Name:5,9-di(phenylsulfonyl)-1-phenylthio-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraene
CAS No.:359010-64-3
Molecular Formula:C₃₈H₄₆O₄S₃
Molecular Weight:662.979
Hs Code.:

Synonyms:5,9-di(phenylsulfonyl)-1-phenylthio-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraene

Suppliers and Price of 5,9-di(phenylsulfonyl)-1-phenylthio-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5,9-di(phenylsulfonyl)-1-phenylthio-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5,9-di(phenylsulfonyl)-1-phenylthio-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraene

There total 7 articles about 5,9-di(phenylsulfonyl)-1-phenylthio-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 359010-59-6
4-bromo-3-methyl-2-butenyl phenyl sulfide

: 359010-62-1
1,5-di(phenylsulfonyl)-3,7,11-trimethyl-2,6,10-dodecatriene

: 359010-64-3
5,9-di(phenylsulfonyl)-1-phenylthio-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraene

Guidance literature:: With n-butyllithium; In tetrahydrofuran; at -78 ℃;
DOI:10.1002/1521-3773(20011001)40:19<3627::AID-ANIE3627>3.0.CO;2-E

Reference yield:

: 57282-70-9
(E)-4-hydroxy-3-methyl-2-butenyl phenyl sulfide

: 359010-64-3
5,9-di(phenylsulfonyl)-1-phenylthio-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraene

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / PBr₃ / diethyl ether

2: 93 percent / n-BuLi / tetrahydrofuran / -78 °C

3: 75 percent / LiNbMoO₆; H₂O₂ / methanol

4: 91 percent / n-BuLi / tetrahydrofuran / -78 °C

With n-butyllithium; LiNbMoO₆; dihydrogen peroxide; phosphorus tribromide; In tetrahydrofuran; methanol; diethyl ether;
DOI:10.1002/1521-3773(20011001)40:19<3627::AID-ANIE3627>3.0.CO;2-E

Reference yield:

: 108-98-5
thiophenol

: 359010-64-3
5,9-di(phenylsulfonyl)-1-phenylthio-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraene

Guidance literature:: Multi-step reaction with 5 steps

1: CuI / dimethylformamide

2: 85 percent / PBr₃ / diethyl ether

3: 93 percent / n-BuLi / tetrahydrofuran / -78 °C

4: 75 percent / LiNbMoO₆; H₂O₂ / methanol

5: 91 percent / n-BuLi / tetrahydrofuran / -78 °C

With copper(l) iodide; n-butyllithium; LiNbMoO₆; dihydrogen peroxide; phosphorus tribromide; In tetrahydrofuran; methanol; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1002/1521-3773(20011001)40:19<3627::AID-ANIE3627>3.0.CO;2-E