1,5,9-tri(phenylsulfonyl)-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraene

Base Information

Chemical Name:1,5,9-tri(phenylsulfonyl)-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraene
CAS No.:359010-65-4
Molecular Formula:C₃₈H₄₆O₆S₃
Molecular Weight:694.978
Hs Code.:

Synonyms:1,5,9-tri(phenylsulfonyl)-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraene

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Chemical Property of 1,5,9-tri(phenylsulfonyl)-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraene

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Technology Process of 1,5,9-tri(phenylsulfonyl)-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraene

There total 9 articles about 1,5,9-tri(phenylsulfonyl)-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 359010-64-3
5,9-di(phenylsulfonyl)-1-phenylthio-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraene

: 359010-65-4
1,5,9-tri(phenylsulfonyl)-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraene

Guidance literature:: With LiNbMoO₆; dihydrogen peroxide; In methanol;
DOI:10.1002/1521-3773(20011001)40:19<3627::AID-ANIE3627>3.0.CO;2-E

Reference yield:

: LiNbMoO₆

: 359010-64-3
5,9-di(phenylsulfonyl)-1-phenylthio-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraene

: 359010-65-4
1,5,9-tri(phenylsulfonyl)-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraene

Guidance literature:: With dihydrogen peroxide; In methanol;

Reference yield:

: 57282-70-9
(E)-4-hydroxy-3-methyl-2-butenyl phenyl sulfide

: 359010-65-4
1,5,9-tri(phenylsulfonyl)-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraene

Guidance literature:: Multi-step reaction with 5 steps

1: 85 percent / PBr₃ / diethyl ether

2: 93 percent / n-BuLi / tetrahydrofuran / -78 °C

3: 75 percent / LiNbMoO₆; H₂O₂ / methanol

4: 91 percent / n-BuLi / tetrahydrofuran / -78 °C

5: 72 percent / LiNbMoO₆; H₂O₂ / methanol

With n-butyllithium; LiNbMoO₆; dihydrogen peroxide; phosphorus tribromide; In tetrahydrofuran; methanol; diethyl ether;
DOI:10.1002/1521-3773(20011001)40:19<3627::AID-ANIE3627>3.0.CO;2-E