4,5-Dihydro-4-isopropyl-1-(4-methyl-2-nitrophenyl)-5-morpholino-1,2,3-triazole

Base Information

Chemical Name:4,5-Dihydro-4-isopropyl-1-(4-methyl-2-nitrophenyl)-5-morpholino-1,2,3-triazole
CAS No.:149179-55-5
Molecular Formula:C₁₆H₂₃N₅O₃
Molecular Weight:333.39
Hs Code.:

Synonyms:4,5-Dihydro-4-isopropyl-1-(4-methyl-2-nitrophenyl)-5-morpholino-1,2,3-triazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,5-Dihydro-4-isopropyl-1-(4-methyl-2-nitrophenyl)-5-morpholino-1,2,3-triazole

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Technology Process of 4,5-Dihydro-4-isopropyl-1-(4-methyl-2-nitrophenyl)-5-morpholino-1,2,3-triazole

There total 1 articles about 4,5-Dihydro-4-isopropyl-1-(4-methyl-2-nitrophenyl)-5-morpholino-1,2,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 110-91-8,99108-56-2
morpholine

: 20615-75-2
4-azido-3-nitro-toluene

: 590-86-3
isovaleraldehyde

: 149179-55-5
4,5-Dihydro-4-isopropyl-1-(4-methyl-2-nitrophenyl)-5-morpholino-1,2,3-triazole

Guidance literature:: In benzene; Ambient temperature;

Reference yield: 83.0%

: 149179-55-5
4,5-Dihydro-4-isopropyl-1-(4-methyl-2-nitrophenyl)-5-morpholino-1,2,3-triazole

: 149179-61-3
1-(2-Amino-4-methylphenyl)-4,5-dihydro-4-isopropyl-5-morpholino-1,2,3-triazole

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; under 760 Torr; Ambient temperature;

Reference yield:

: 149179-55-5
4,5-Dihydro-4-isopropyl-1-(4-methyl-2-nitrophenyl)-5-morpholino-1,2,3-triazole

: 2-Isopropyl-6-methylquinoxaline

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / H₂ / 10percent Pd/C / ethanol / 760 Torr / Ambient temperature

2: 2) 2,3-dichloro-5,6-dicyanobenzoquinone / 1) toluene, reflux, 1 h, 2) THF, RT, 3-6 h

With hydrogen; 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium on activated charcoal; In ethanol;