3-Nitro-4-azidotoluene

Base Information

Chemical Name:3-Nitro-4-azidotoluene
CAS No.:20615-75-2
Molecular Formula:C₇H₆N₄O₂
Molecular Weight:178.15
Hs Code.:
Mol file:20615-75-2.mol

Synonyms:4-azido-3-nitro-toluene

Suppliers and Price of 3-Nitro-4-azidotoluene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
1-azido-4-methyl-2-nitrobenzene
50mg
$ 90.00

AK Scientific
4-Methyl-2-nitrophenylazide
500mg
$ 409.00

Total 1 raw suppliers

Chemical Property of 3-Nitro-4-azidotoluene

Chemical Property:

Purity/Quality:: 1-azido-4-methyl-2-nitrobenzene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Nitro-4-azidotoluene

There total 6 articles about 3-Nitro-4-azidotoluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106-49-0,12221-03-3
p-toluidine

: 20615-75-2
4-azido-3-nitro-toluene

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid / 0.25 h / Heating

2: 60percent nitric acid, conc. sulfuric acid / 1.) 0 deg C, 10 min, 2.) RT, 30 min

3: conc. sulfuric acid / 0.25 h / 100 °C

4: 1.) aq. HCl, NaNO₂, 2.) aq. NaN₃, sodium acetate / 1.) 0 deg C, 15 min

With hydrogenchloride; sodium azide; sulfuric acid; nitric acid; sodium acetate; sodium nitrite; In acetic acid;
DOI:10.1021/jm00010a023

Reference yield:

: 612-45-3
4-methyl-2-nitroacetanilide

: 20615-75-2
4-azido-3-nitro-toluene

Guidance literature:: Multi-step reaction with 2 steps

1: conc. sulfuric acid / 0.25 h / 100 °C

2: 1.) aq. HCl, NaNO₂, 2.) aq. NaN₃, sodium acetate / 1.) 0 deg C, 15 min

With hydrogenchloride; sodium azide; sulfuric acid; sodium acetate; sodium nitrite;
DOI:10.1021/jm00010a023

Reference yield:

: 103-89-9
4-Methylacetanilide

: 20615-75-2
4-azido-3-nitro-toluene

Guidance literature:: Multi-step reaction with 3 steps

1: 60percent nitric acid, conc. sulfuric acid / 1.) 0 deg C, 10 min, 2.) RT, 30 min

2: conc. sulfuric acid / 0.25 h / 100 °C

3: 1.) aq. HCl, NaNO₂, 2.) aq. NaN₃, sodium acetate / 1.) 0 deg C, 15 min

With hydrogenchloride; sodium azide; sulfuric acid; nitric acid; sodium acetate; sodium nitrite;
DOI:10.1021/jm00010a023