2-acetamido-5-O-acetyl-1,3,6-tris-O-t-butyldiphenylsilyl-2-deoxy-β-D-glucofuranose

Base Information

Chemical Name:2-acetamido-5-O-acetyl-1,3,6-tris-O-t-butyldiphenylsilyl-2-deoxy-β-D-glucofuranose
CAS No.:741672-25-3
Molecular Formula:C₅₈H₇₁NO₇Si₃
Molecular Weight:978.461
Hs Code.:

Synonyms:2-acetamido-5-O-acetyl-1,3,6-tris-O-t-butyldiphenylsilyl-2-deoxy-β-D-glucofuranose

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Chemical Property of 2-acetamido-5-O-acetyl-1,3,6-tris-O-t-butyldiphenylsilyl-2-deoxy-β-D-glucofuranose

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Technology Process of 2-acetamido-5-O-acetyl-1,3,6-tris-O-t-butyldiphenylsilyl-2-deoxy-β-D-glucofuranose

There total 5 articles about 2-acetamido-5-O-acetyl-1,3,6-tris-O-t-butyldiphenylsilyl-2-deoxy-β-D-glucofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 741672-22-0
2-acetamido-1,3,6-tris-O-t-butyldiphenylsilyl-4-chloromethylsulfonyl-2-deoxy-β-D-glucopyranose

: 3396-11-0
cesium acetate

: 741672-25-3
2-acetamido-5-O-acetyl-1,3,6-tris-O-t-butyldiphenylsilyl-2-deoxy-β-D-glucofuranose

Guidance literature:: With 18-crown-6 ether; In toluene; at 120 ℃; for 4h;
DOI:10.1246/bcsj.77.1181

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 741672-25-3
2-acetamido-5-O-acetyl-1,3,6-tris-O-t-butyldiphenylsilyl-2-deoxy-β-D-glucofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / imidazole / dimethylformamide / 47 h / 20 °C

2: 72 percent / Et₃N / diethyl ether / 3 h / 20 °C

3: 69 percent / 18-crown-6 / toluene / 4 h / 120 °C

With 1H-imidazole; 18-crown-6 ether; triethylamine; In diethyl ether; N,N-dimethyl-formamide; toluene;
DOI:10.1246/bcsj.77.1181

Reference yield:

: 741672-19-5
2-acetamido-1,3,6-tris-O-t-butyldiphenylsilyl-2-deoxy-β-D-glucopyranose

: 741672-25-3
2-acetamido-5-O-acetyl-1,3,6-tris-O-t-butyldiphenylsilyl-2-deoxy-β-D-glucofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / Et₃N / diethyl ether / 3 h / 20 °C

2: 69 percent / 18-crown-6 / toluene / 4 h / 120 °C

With 18-crown-6 ether; triethylamine; In diethyl ether; toluene;
DOI:10.1246/bcsj.77.1181