2-acetamido-1,3,6-tris-O-t-butyldiphenylsilyl-4-chloromethylsulfonyl-2-deoxy-β-D-glucopyranose

Base Information

Chemical Name:2-acetamido-1,3,6-tris-O-t-butyldiphenylsilyl-4-chloromethylsulfonyl-2-deoxy-β-D-glucopyranose
CAS No.:741672-22-0
Molecular Formula:C₅₇H₇₀ClNO₈SSi₃
Molecular Weight:1048.96
Hs Code.:

Synonyms:2-acetamido-1,3,6-tris-O-t-butyldiphenylsilyl-4-chloromethylsulfonyl-2-deoxy-β-D-glucopyranose

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Chemical Property of 2-acetamido-1,3,6-tris-O-t-butyldiphenylsilyl-4-chloromethylsulfonyl-2-deoxy-β-D-glucopyranose

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Technology Process of 2-acetamido-1,3,6-tris-O-t-butyldiphenylsilyl-4-chloromethylsulfonyl-2-deoxy-β-D-glucopyranose

There total 4 articles about 2-acetamido-1,3,6-tris-O-t-butyldiphenylsilyl-4-chloromethylsulfonyl-2-deoxy-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 741672-19-5
2-acetamido-1,3,6-tris-O-t-butyldiphenylsilyl-2-deoxy-β-D-glucopyranose

: 3518-65-8
monochloromethanesulfonyl chloride

: 741672-22-0
2-acetamido-1,3,6-tris-O-t-butyldiphenylsilyl-4-chloromethylsulfonyl-2-deoxy-β-D-glucopyranose

Guidance literature:: With triethylamine; In diethyl ether; at 20 ℃; for 3h;
DOI:10.1246/bcsj.77.1181

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 741672-22-0
2-acetamido-1,3,6-tris-O-t-butyldiphenylsilyl-4-chloromethylsulfonyl-2-deoxy-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / imidazole / dimethylformamide / 47 h / 20 °C

2: 72 percent / Et₃N / diethyl ether / 3 h / 20 °C

With 1H-imidazole; triethylamine; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.77.1181

Reference yield:

: 741672-17-3
2-acetamido-1,4,6-tris-O-t-butyldiphenylsilyl-2-deoxy-β-D-glucopyranose

: 741672-22-0
2-acetamido-1,3,6-tris-O-t-butyldiphenylsilyl-4-chloromethylsulfonyl-2-deoxy-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 39 percent / NaOH / H₂O; ethanol

2: 72 percent / Et₃N / diethyl ether / 3 h / 20 °C

With sodium hydroxide; triethylamine; In diethyl ether; ethanol; water;
DOI:10.1246/bcsj.77.1181