5-phthalimido-2-oxopentaldehyde bis[4-(4-chlorophenyl)-3-thiosemicarbazide]

Base Information

Chemical Name:5-phthalimido-2-oxopentaldehyde bis[4-(4-chlorophenyl)-3-thiosemicarbazide]
CAS No.:1252573-64-0
Molecular Formula:C₂₇H₂₃Cl₂N₇O₂S₂
Molecular Weight:612.563
Hs Code.:

Synonyms:5-phthalimido-2-oxopentaldehyde bis[4-(4-chlorophenyl)-3-thiosemicarbazide]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-phthalimido-2-oxopentaldehyde bis[4-(4-chlorophenyl)-3-thiosemicarbazide]

Chemical Property:

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Technology Process of 5-phthalimido-2-oxopentaldehyde bis[4-(4-chlorophenyl)-3-thiosemicarbazide]

There total 6 articles about 5-phthalimido-2-oxopentaldehyde bis[4-(4-chlorophenyl)-3-thiosemicarbazide] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22814-92-2
4-(p-chlorophenyl)-3-thiosemicarbazide

: C₁₃H₁₁NO₄

: 1252573-64-0
5-phthalimido-2-oxopentaldehyde bis[4-(4-chlorophenyl)-3-thiosemicarbazide]

Guidance literature:: In ethanol; water; Reflux;
DOI:10.1248/cpb.58.208

Reference yield:

: 3130-75-4
4-phthalimidobutyric acid

: 1252573-64-0
5-phthalimido-2-oxopentaldehyde bis[4-(4-chlorophenyl)-3-thiosemicarbazide]

Guidance literature:: Multi-step reaction with 5 steps

1: thionyl chloride / Reflux

2: potassium hydroxide / diethyl ether; water / 0.17 h

3: hydrogen bromide / water; tetrahydrofuran

4: dimethyl sulfoxide / 2 h / 80 °C

5: ethanol / 2 h / Reflux

With thionyl chloride; hydrogen bromide; dimethyl sulfoxide; potassium hydroxide; In tetrahydrofuran; diethyl ether; ethanol; water;

Reference yield:

: 84461-00-7
1-diazo-5-phthalimido-2-pentanone

: 1252573-64-0
5-phthalimido-2-oxopentaldehyde bis[4-(4-chlorophenyl)-3-thiosemicarbazide]

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen bromide / water; tetrahydrofuran

2: dimethyl sulfoxide / 2 h / 80 °C

3: ethanol / 2 h / Reflux

With hydrogen bromide; dimethyl sulfoxide; In tetrahydrofuran; ethanol; water;