1,4-bis(mercapto ethyloxy ethyloxy ethyl)benzene

Base Information

• Chemical Name: 1,4-bis(mercapto ethyloxy ethyloxy ethyl)benzene
• CAS No.: 111530-51-9
• Molecular Formula: C₁₈H₃₀O₆S₂
• Molecular Weight: 406.565
• Mol file: 111530-51-9.mol

Synonyms:1,4-bis(mercapto ethyloxy ethyloxy ethyl)benzene

Chemical Property of 1,4-bis(mercapto ethyloxy ethyloxy ethyl)benzene

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 1,4-bis(mercapto ethyloxy ethyloxy ethyl)benzene

There total 7 articles about 1,4-bis(mercapto ethyloxy ethyloxy ethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

triethylene glycol di-(p-toluenesulfonate) (19249-03-7) → 1,4-bis(mercapto ethyloxy ethyloxy ethyl)benzene (111530-51-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 46 percent / K₂CO₃ / acetonitrile / 168 h / Heating

2: 1 g / dimethylformamide / 168 h / 20 °C

3: NaOMe / methanol / 0.08 h

With sodium methylate; potassium carbonate; In methanol; N,N-dimethyl-formamide; acetonitrile;

DOI:10.1021/jp022102c

Reference yield:

1,4-bis(thioacetate ethyl oxyethyl oxyethyl)benzene (490022-52-1) → 1,4-bis(mercapto ethyloxy ethyloxy ethyl)benzene (111530-51-9)

Guidance literature:

With sodium methylate; In methanol; for 0.0833333h;

DOI:10.1021/jp022102c

Reference yield:

1,4-bis[2-(2-(2-(p-toluenesulfonylethoxy)-ethoxy)ethoxy)]benzene (134881-73-5) → 1,4-bis(mercapto ethyloxy ethyloxy ethyl)benzene (111530-51-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1 g / dimethylformamide / 168 h / 20 °C

2: NaOMe / methanol / 0.08 h

With sodium methylate; In methanol; N,N-dimethyl-formamide;

DOI:10.1021/jp022102c

upstream raw materials:

1,4-bis{2-[2-(2-bromoethoxy)ethoxy]ethoxy}benzene

thiourea

1,4-bis(thioacetate ethyl oxyethyl oxyethyl)benzene

1,4-bis[2-(2-(2-(p-toluenesulfonylethoxy)-ethoxy)ethoxy)]benzene