1,4-bis(thioacetate ethyl oxyethyl oxyethyl)benzene

Base Information

• Chemical Name: 1,4-bis(thioacetate ethyl oxyethyl oxyethyl)benzene
• CAS No.: 490022-52-1
• Molecular Formula: C₂₂H₃₄O₈S₂
• Molecular Weight: 490.639
• Mol file: 490022-52-1.mol

Synonyms:1,4-bis(thioacetate ethyl oxyethyl oxyethyl)benzene

Chemical Property of 1,4-bis(thioacetate ethyl oxyethyl oxyethyl)benzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,4-bis(thioacetate ethyl oxyethyl oxyethyl)benzene

There total 3 articles about 1,4-bis(thioacetate ethyl oxyethyl oxyethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

triethylene glycol di-(p-toluenesulfonate) (19249-03-7) → 1,4-bis(thioacetate ethyl oxyethyl oxyethyl)benzene (490022-52-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 46 percent / K₂CO₃ / acetonitrile / 168 h / Heating

2: 1 g / dimethylformamide / 168 h / 20 °C

With potassium carbonate; In N,N-dimethyl-formamide; acetonitrile;

DOI:10.1021/jp022102c

Reference yield:

hydroquinone (123-31-9,8027-02-9) → 1,4-bis(thioacetate ethyl oxyethyl oxyethyl)benzene (490022-52-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 46 percent / K₂CO₃ / acetonitrile / 168 h / Heating

2: 1 g / dimethylformamide / 168 h / 20 °C

With potassium carbonate; In N,N-dimethyl-formamide; acetonitrile;

DOI:10.1021/jp022102c

Reference yield:

(R)-thioacetate (29632-72-2) + 1,4-bis[2-(2-(2-(p-toluenesulfonylethoxy)-ethoxy)ethoxy)]benzene (134881-73-5) → 1,4-bis(thioacetate ethyl oxyethyl oxyethyl)benzene (490022-52-1)

Guidance literature:

In N,N-dimethyl-formamide; at 20 ℃; for 168h;

DOI:10.1021/jp022102c

upstream raw materials:

(R)-thioacetate

1,4-bis[2-(2-(2-(p-toluenesulfonylethoxy)-ethoxy)ethoxy)]benzene

hydroquinone

triethylene glycol di-(p-toluenesulfonate)

Downstream raw materials:

1,4-bis(mercapto ethyloxy ethyloxy ethyl)benzene