(2E)-3-<2-<10-(2-Formylphenoxy)decyloxy>phenyl>-2-propensaeure-methylester

Base Information

• Chemical Name: (2E)-3-<2-<10-(2-Formylphenoxy)decyloxy>phenyl>-2-propensaeure-methylester
• CAS No.: 345254-33-3
• Molecular Formula: C₂₇H₃₄O₅
• Molecular Weight: 438.564
• Mol file: 345254-33-3.mol

Synonyms:(2E)-3-<2-<10-(2-Formylphenoxy)decyloxy>phenyl>-2-propensaeure-methylester

Chemical Property of (2E)-3-<2-<10-(2-Formylphenoxy)decyloxy>phenyl>-2-propensaeure-methylester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (2E)-3-<2-<10-(2-Formylphenoxy)decyloxy>phenyl>-2-propensaeure-methylester

There total 5 articles about (2E)-3-<2-<10-(2-Formylphenoxy)decyloxy>phenyl>-2-propensaeure-methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

trimethyl phosphonoacetate (5927-18-4) + 2,2’-[decane-1,10-diylbis(oxy)]dibenzaldehyde (70185-70-5) → (2E)-3-<2-<10-(2-Formylphenoxy)decyloxy>phenyl>-2-propensaeure-methylester (345254-33-3)

Guidance literature:

With sodium hydride; In benzene; for 6h; Ambient temperature;

Reference yield: 68.0%

salicylaldehyde (90-02-8) + (2E)-3-<2-(10-Bromdecyloxy)phenyl>-2-propensaeure-methylester (344902-60-9) → (2E)-3-<2-<10-(2-Formylphenoxy)decyloxy>phenyl>-2-propensaeure-methylester (345254-33-3)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; for 48h;

Reference yield:

salicylaldehyde (90-02-8) → (2E)-3-<2-<10-(2-Formylphenoxy)decyloxy>phenyl>-2-propensaeure-methylester (345254-33-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 9.7 percent / K₂CO₃ / dimethylformamide / 24 h

2: 85 percent / NaH / benzene / 6 h / Ambient temperature

With sodium hydride; potassium carbonate; In N,N-dimethyl-formamide; benzene;

upstream raw materials:

trimethyl phosphonoacetate

2,2’-[decane-1,10-diylbis(oxy)]dibenzaldehyde

salicylaldehyde

(2E)-3-<2-(10-Bromdecyloxy)phenyl>-2-propensaeure-methylester

Downstream raw materials:

diphenylfumaronitrile

(2E)-3-<2-<10-<2-(3-Cyan-trans-3-phenyl-2-oxiranyl)phenoxy>decyloxy>phenyl>-2-propensaeure-methylester