2-methanesulfonyl-4-piperidin-4-yl-phenylamine; compound with acetic acid

Base Information

• Chemical Name: 2-methanesulfonyl-4-piperidin-4-yl-phenylamine; compound with acetic acid
• CAS No.: 1037299-79-8
• Molecular Formula: C₂H₄O₂*C₁₂H₁₈N₂O₂S
• Molecular Weight: 314.406

Synonyms:2-methanesulfonyl-4-piperidin-4-yl-phenylamine; compound with acetic acid

Chemical Property of 2-methanesulfonyl-4-piperidin-4-yl-phenylamine; compound with acetic acid

Chemical Property:

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Technology Process of 2-methanesulfonyl-4-piperidin-4-yl-phenylamine; compound with acetic acid

There total 1 articles about 2-methanesulfonyl-4-piperidin-4-yl-phenylamine; compound with acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methanesulfonyl-4-pyridin-4-yl-phenylamine (1037299-77-6) + acetic acid (64-19-7,77671-22-8) → 2-methanesulfonyl-4-piperidin-4-yl-phenylamine; compound with acetic acid (1037299-79-8)

Guidance literature:

With hydrogen; platinum(IV) oxide; at 80 ℃; for 8h; under 825.083 Torr;

Reference yield:

2-methanesulfonyl-4-piperidin-4-yl-phenylamine; compound with acetic acid (1037299-79-8) + di-tert-butyl dicarbonate (24424-99-5) → 4-(4-amino-3-methanesulfonyl-phenyl)-piperidine-1-carboxylic acid tert-butyl ester (1037299-80-1)

Guidance literature:

With sodium carbonate; In dichloromethane; water; at 20 ℃; for 3h;

upstream raw materials:

2-methanesulfonyl-4-pyridin-4-yl-phenylamine

acetic acid

Downstream raw materials:

4-(4-amino-3-methanesulfonyl-phenyl)-piperidine-1-carboxylic acid tert-butyl ester

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