N-[[1-[(2-Furanylcarbonyl)amino]cyclohexyl]carbonyl]-L-valine ethyl ester

Base Information

Chemical Name:N-[[1-[(2-Furanylcarbonyl)amino]cyclohexyl]carbonyl]-L-valine ethyl ester
CAS No.:944281-98-5
Molecular Formula:C₁₉H₂₈N₂O₅
Molecular Weight:364.442
Hs Code.:

Synonyms:N-[[1-[(2-Furanylcarbonyl)amino]cyclohexyl]carbonyl]-L-valine ethyl ester

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Chemical Property of N-[[1-[(2-Furanylcarbonyl)amino]cyclohexyl]carbonyl]-L-valine ethyl ester

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Technology Process of N-[[1-[(2-Furanylcarbonyl)amino]cyclohexyl]carbonyl]-L-valine ethyl ester

There total 4 articles about N-[[1-[(2-Furanylcarbonyl)amino]cyclohexyl]carbonyl]-L-valine ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 944281-51-0
2-(2-furanyl)-3-oxa-1-azaspiro[4.5]dec-1-en-4-one

: 17609-47-1
L-Valine ethyl ester hydrochloride

: 944281-98-5
N-[[1-[(2-Furanylcarbonyl)amino]cyclohexyl]carbonyl]-L-valine ethyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; for 72h;

Reference yield:

: 63203-41-8
1-(furan-2-carboxamido)-cyclohexanecarboxylic acid

: 944281-98-5
N-[[1-[(2-Furanylcarbonyl)amino]cyclohexyl]carbonyl]-L-valine ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; isobutyl chloroformate / tetrahydrofuran / 1 h / 20 °C

2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 72 h

With triethylamine; N-ethyl-N,N-diisopropylamine; isobutyl chloroformate; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 2756-85-6
1-aminocyclohexane carboxylic acid

: 944281-98-5
N-[[1-[(2-Furanylcarbonyl)amino]cyclohexyl]carbonyl]-L-valine ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / water / 2 h / 80 °C

1.2: 0 - 20 °C

1.3: 0 °C

2.1: triethylamine; isobutyl chloroformate / tetrahydrofuran / 1 h / 20 °C

3.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 72 h

With sodium hydroxide; triethylamine; N-ethyl-N,N-diisopropylamine; isobutyl chloroformate; In tetrahydrofuran; water; N,N-dimethyl-formamide;