[18F]fluoromethylene toluene-4-sulfonate

Base Information

Chemical Name:[18F]fluoromethylene toluene-4-sulfonate
CAS No.:113426-16-7
Molecular Formula:C₈H₉FO₃S
Molecular Weight:203.224
Hs Code.:

Synonyms:[18F]fluoromethylene toluene-4-sulfonate

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Chemical Property of [18F]fluoromethylene toluene-4-sulfonate

Chemical Property:

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Technology Process of [18F]fluoromethylene toluene-4-sulfonate

There total 3 articles about [18F]fluoromethylene toluene-4-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 24124-59-2
methylene ditosylate

: 113426-16-7
[18F]fluoromethylene toluene-4-sulfonate

Guidance literature:: With potassium carbonate; [2.2.2]cryptande; [18F]fluoride ion, cyclotron produced, NCA; In water; acetonitrile; at 120 ℃; for 0.166667h; Inert atmosphere; Sealed tube;
DOI:10.1016/j.ejmech.2016.04.036

Reference yield:

: 15310-28-8
bis(4-methylphenylsulfonyl)methane

: 113426-16-7
[18F]fluoromethylene toluene-4-sulfonate

Guidance literature:: With potassium carbonate; In acetonitrile; at 110 ℃; for 0.0833333h;

Reference yield:

: 16836-95-6
silver(I) 4-methylbenzenesulfonate

: 113426-16-7
[18F]fluoromethylene toluene-4-sulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetonitrile / 16 h / Reflux

2.1: K_2.2.2/K¹⁸F / acetonitrile; water / 0.17 h

2.2: 0.08 h / 80 °C

With K_2.2.2/K¹⁸F; In water; acetonitrile;
DOI:10.1039/c9cc04901k