N-benzyl-1-(pyren-1-yl)methanaminium

Base Information

Chemical Name:N-benzyl-1-(pyren-1-yl)methanaminium
CAS No.:127856-78-4
Molecular Formula:C₂₄H₁₉N
Molecular Weight:321.422
Hs Code.:

Synonyms:N-benzyl-1-(pyren-1-yl)methanaminium

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Chemical Property of N-benzyl-1-(pyren-1-yl)methanaminium

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Technology Process of N-benzyl-1-(pyren-1-yl)methanaminium

There total 1 articles about N-benzyl-1-(pyren-1-yl)methanaminium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3029-19-4
pyrene-1-aldehyde

: 100-46-9
benzylamine

: 127856-78-4
N-benzyl-1-(pyren-1-yl)methanaminium

Guidance literature:: With hydrogenchloride; sodium cyanoborohydride; toluene-4-sulfonic acid; Yield given. Multistep reaction; 1.) toluene, reflux, 2.) EtOH, RT, pH 6-7, 2-3 d;
DOI:10.1021/jm00171a012

Reference yield: 83.2%

: 75-15-0,12122-00-8
carbon disulfide

: 1135-99-5
diphenyltin(IV) dichloride

: 127856-78-4
N-benzyl-1-(pyren-1-yl)methanaminium

: 1357011-39-2
S₂CN(CH₂C₆H₅)(CH₂C₁₆H₉)SnCl(C₆H₅)2

Guidance literature:: With NaOH; In tetrahydrofuran; methanol; to soln. of amine, NaOH (THF, MeOH) CS2 added; mixt. stirred at 20°C for 12 h; soln. Ph2SnCl2 (MeOH) added; stirred at 20°C for 5 h; ppt. collected by filtration; elem. anal.;;
DOI:10.1016/j.poly.2011.11.022