(2S,3R)-4-methylene-2-((E)-styryl)-1-((S)-toluene-4-sulfinyl)-pyrrolidine-3-carboxylic acid diphenylamide

Base Information

Chemical Name:(2S,3R)-4-methylene-2-((E)-styryl)-1-((S)-toluene-4-sulfinyl)-pyrrolidine-3-carboxylic acid diphenylamide
CAS No.:1073146-81-2
Molecular Formula:C₃₃H₃₀N₂O₂S
Molecular Weight:518.679
Hs Code.:

Synonyms:(2S,3R)-4-methylene-2-((E)-styryl)-1-((S)-toluene-4-sulfinyl)-pyrrolidine-3-carboxylic acid diphenylamide

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Chemical Property of (2S,3R)-4-methylene-2-((E)-styryl)-1-((S)-toluene-4-sulfinyl)-pyrrolidine-3-carboxylic acid diphenylamide

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Technology Process of (2S,3R)-4-methylene-2-((E)-styryl)-1-((S)-toluene-4-sulfinyl)-pyrrolidine-3-carboxylic acid diphenylamide

There total 1 articles about (2S,3R)-4-methylene-2-((E)-styryl)-1-((S)-toluene-4-sulfinyl)-pyrrolidine-3-carboxylic acid diphenylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 153277-52-2
(S)-(+)-N-((2E)-3-phenylprop-2-enylidene)-p-toluenesulfinamide

: 440084-59-3
2-methylene-cyclopropanecarboxylic acid diphenyl amide

: 1073146-81-2
(2S,3R)-4-methylene-2-((E)-styryl)-1-((S)-toluene-4-sulfinyl)-pyrrolidine-3-carboxylic acid diphenylamide

: (2R,3S)-4-methylene-2-((E)-styryl)-1-((S)-toluene-4-sulfinyl)-pyrrolidine-3-carboxylic acid diphenylamide

: cis-4-methylene-2-((E)-styryl)-1-((S)-toluene-4-sulfinyl)-pyrrolidine-3-carboxylic acid diphenylamide

Guidance literature:: With magnesium iodide; In tetrahydrofuran; at 20 ℃; for 10.3333h; optical yield given as %de; stereoselective reaction; Inert atmosphere; Reflux;
DOI:10.1021/jo802049u

Reference yield: 94.0%

: 1073146-81-2
(2S,3R)-4-methylene-2-((E)-styryl)-1-((S)-toluene-4-sulfinyl)-pyrrolidine-3-carboxylic acid diphenylamide

: 1073147-02-0
(2S,3R)-4-methylene-2-((E)-styryl)-pyrrolidine-3-carboxylic acid diphenylamide

Guidance literature:: (2S,3R)-4-methylene-2-((E)-styryl)-1-((S)-toluene-4-sulfinyl)-pyrrolidine-3-carboxylic acid diphenylamide; With methanol; trifluoroacetic acid; at 0 - 20 ℃; for 3h; Inert atmosphere;

With sodium hydrogencarbonate; In methanol; water; at 20 ℃; Inert atmosphere; Saturated solution;
DOI:10.1021/jo802049u