3-thiophenecarboxylic acid phenyl ester

Base Information

Chemical Name:3-thiophenecarboxylic acid phenyl ester
CAS No.:14596-83-9
Molecular Formula:C₁₁H₈O₂S
Molecular Weight:204.249
Hs Code.:

Synonyms:3-thiophenecarboxylic acid phenyl ester

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Chemical Property of 3-thiophenecarboxylic acid phenyl ester

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Technology Process of 3-thiophenecarboxylic acid phenyl ester

There total 10 articles about 3-thiophenecarboxylic acid phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 10486-61-0
3-thienyl iodide

: 1864-94-4
phenyl formate

: 14596-83-9
3-thiophenecarboxylic acid phenyl ester

Guidance literature:: With palladium diacetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In acetonitrile; at 20 ℃; for 6h;
DOI:10.1002/adsc.201700751

Reference yield: 95.0%

: 872-31-1
3-Bromothiophene

: 1864-94-4
phenyl formate

: 14596-83-9
3-thiophenecarboxylic acid phenyl ester

Guidance literature:: With palladium diacetate; triethylamine; tri tert-butylphosphoniumtetrafluoroborate; In acetonitrile; at 80 ℃; Inert atmosphere;
DOI:10.1021/ol301192s

Reference yield: 89.0%

: 872-31-1
3-Bromothiophene

: 13939-06-5,199620-15-0
molybdenum hexacarbonyl

: 108-95-2,27073-41-2
phenol

: 14596-83-9
3-thiophenecarboxylic acid phenyl ester

Guidance literature:: With tributyl-amine; In diethylene glycol dimethyl ether; at 150 ℃; for 12h; Inert atmosphere;
DOI:10.1055/s-0030-1260060