10-undecyn-1-yl N-phenylcarbamate

Base Information

• Chemical Name: 10-undecyn-1-yl N-phenylcarbamate
• CAS No.: 478404-25-0
• Molecular Formula: C₁₈H₂₅NO₂
• Molecular Weight: 287.402
• Mol file: 478404-25-0.mol

Synonyms:10-undecyn-1-yl N-phenylcarbamate

Chemical Property of 10-undecyn-1-yl N-phenylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 10-undecyn-1-yl N-phenylcarbamate

There total 3 articles about 10-undecyn-1-yl N-phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

undec-10-yn-1-ol (2774-84-7) + phenyl isocyanate (103-71-9) → 10-undecyn-1-yl N-phenylcarbamate (478404-25-0)

Guidance literature:

With 1,2-bis{(2-ethylhexanoyl)oxy}dibutylstannane; triethylamine; In tetrahydrofuran; for 2h;

DOI:10.1023/A:1020326818084

Reference yield:

undec-10-ynoic acid (2777-65-3) → 10-undecyn-1-yl N-phenylcarbamate (478404-25-0)

Guidance literature:

Multi-step reaction with 3 steps

1: HCl / zuletzt bei Siedetemperatur

2: sodium; butyl alcohol

With hydrogenchloride; sodium; butan-1-ol;

Reference yield:

ethyl ester of dodec-11-ynoic acid (94030-75-8) → 10-undecyn-1-yl N-phenylcarbamate (478404-25-0)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium; butyl alcohol

With sodium; butan-1-ol;

upstream raw materials:

undec-10-yn-1-ol

phenyl isocyanate

undec-10-ynoic acid

ethyl ester of dodec-11-ynoic acid

Downstream raw materials:

10,12-docosadiyne-1,22-diyl bis-N-phenylcarbamate