C₂₂H₂₃ClN₄

Base Information

Chemical Name:C₂₂H₂₃ClN₄
CAS No.:1398546-28-5
Molecular Formula:C₂₂H₂₃ClN₄
Molecular Weight:378.904
Hs Code.:

C<sub>22</sub>H<sub>23</sub>ClN<sub>4</sub>

Synonyms:C₂₂H₂₃ClN₄

Suppliers and Price of C₂₂H₂₃ClN₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₂H₂₃ClN₄

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₂H₂₃ClN₄

There total 9 articles about C₂₂H₂₃ClN₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1376918-13-6
8-amino-3-benzylamino-6-chloro-9H-β-carboline

: 75-07-0,9002-91-9
acetaldehyde

: 1398546-28-5
C₂₂H₂₃ClN₄

Guidance literature:: 8-amino-3-benzylamino-6-chloro-9H-β-carboline; acetaldehyde; With sodium methylate; In methanol; for 2h; Reflux; Inert atmosphere;

With sodium tetrahydroborate; In methanol; at 0 ℃; for 1h; Reflux; Inert atmosphere;
DOI:10.1016/j.bmcl.2012.03.077

Reference yield:

: 1376918-23-8
3-amino-6-chloro-9H-β-carboline

: 1398546-28-5
C₂₂H₂₃ClN₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: chloroform / 0.5 h / 40 °C / Inert atmosphere

2.1: sodium nitrate; trifluoroacetic acid / 18 h / 0 - 20 °C / Inert atmosphere

3.1: hydrogenchloride / water / 12 h / Reflux; Inert atmosphere

4.1: acetic acid / methanol / 4 h / 20 °C / pH 4 / Inert atmosphere

5.1: sodium cyanoborohydride / methanol / 1 h / 20 °C / Inert atmosphere

6.1: hydrogenchloride; tin(II) chloride dihdyrate / methanol; water / 48 h / 0 - 20 °C / Inert atmosphere

7.1: sodium methylate / methanol / 2 h / Reflux; Inert atmosphere

7.2: 1 h / 0 °C / Reflux; Inert atmosphere

With hydrogenchloride; sodium nitrate; tin(II) chloride dihdyrate; sodium methylate; sodium cyanoborohydride; acetic acid; trifluoroacetic acid; In methanol; chloroform; water;
DOI:10.1016/j.bmcl.2012.03.077

Reference yield:

: 69954-48-9
methyl 9H-β-carboline-3-carboxylate

: 1398546-28-5
C₂₂H₂₃ClN₄

Guidance literature:: Multi-step reaction with 11 steps

1.1: N-chloro-succinimide / ethyl acetate / 18 h / Inert atmosphere; Reflux

2.1: hydrazine hydrate / pentan-1-ol / 7 h / Reflux; Inert atmosphere

3.1: hydrogenchloride; sodium nitrite / water / 2 h / 0 °C / Inert atmosphere

4.1: acetic acid / water / 1 h / Reflux; Inert atmosphere

5.1: chloroform / 0.5 h / 40 °C / Inert atmosphere

6.1: sodium nitrate; trifluoroacetic acid / 18 h / 0 - 20 °C / Inert atmosphere

7.1: hydrogenchloride / water / 12 h / Reflux; Inert atmosphere

8.1: acetic acid / methanol / 4 h / 20 °C / pH 4 / Inert atmosphere

9.1: sodium cyanoborohydride / methanol / 1 h / 20 °C / Inert atmosphere

10.1: hydrogenchloride; tin(II) chloride dihdyrate / methanol; water / 48 h / 0 - 20 °C / Inert atmosphere

11.1: sodium methylate / methanol / 2 h / Reflux; Inert atmosphere

11.2: 1 h / 0 °C / Reflux; Inert atmosphere

With hydrogenchloride; sodium nitrate; N-chloro-succinimide; tin(II) chloride dihdyrate; sodium methylate; sodium cyanoborohydride; hydrazine hydrate; acetic acid; trifluoroacetic acid; sodium nitrite; In methanol; pentan-1-ol; chloroform; water; ethyl acetate; 4.1: Curtius rearrangement;
DOI:10.1016/j.bmcl.2012.03.077