methyl 4,5,7-tri-O-benzyl-2,3-O-isopropylidene-α-D-gluco-hept-2-ulopyranosonate

Base Information

Chemical Name:methyl 4,5,7-tri-O-benzyl-2,3-O-isopropylidene-α-D-gluco-hept-2-ulopyranosonate
CAS No.:136305-64-1
Molecular Formula:C₃₂H₃₆O₈
Molecular Weight:548.633
Hs Code.:

Synonyms:methyl 4,5,7-tri-O-benzyl-2,3-O-isopropylidene-α-D-gluco-hept-2-ulopyranosonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4,5,7-tri-O-benzyl-2,3-O-isopropylidene-α-D-gluco-hept-2-ulopyranosonate

Chemical Property:

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Technology Process of methyl 4,5,7-tri-O-benzyl-2,3-O-isopropylidene-α-D-gluco-hept-2-ulopyranosonate

There total 3 articles about methyl 4,5,7-tri-O-benzyl-2,3-O-isopropylidene-α-D-gluco-hept-2-ulopyranosonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 136305-59-4
methyl 4,5,7-tri-O-benzyl-α-D-gluco-hept-2-ulopyranosonate

: 77-76-9
2,2-dimethoxy-propane

: 136305-64-1
methyl 4,5,7-tri-O-benzyl-2,3-O-isopropylidene-α-D-gluco-hept-2-ulopyranosonate

Guidance literature:: With hydrogenchloride; In toluene; at 0 ℃; for 0.0833333h;

Reference yield:

: 127994-68-7
methyl onate

: 136305-64-1
methyl 4,5,7-tri-O-benzyl-2,3-O-isopropylidene-α-D-gluco-hept-2-ulopyranosonate

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / 200 °C / vacuum

2: 92 percent / osmium tetroxide, N-methylmorpholine-N-oxide / 2-methyl-propan-2-ol

3: 76 percent / HCl

With hydrogenchloride; osmium(VIII) oxide; 4-methylmorpholine N-oxide; In tert-butyl alcohol;
DOI:10.1016/S0040-4039(00)78786-7

Reference yield:

: 110390-66-4
methyl (4R,5S,6R)-4,5-bis(benzyloxy)-6-(benzyloxymethyl)-5,6-dihydro-4H-pyran-2-carboxylate

: 136305-64-1
methyl 4,5,7-tri-O-benzyl-2,3-O-isopropylidene-α-D-gluco-hept-2-ulopyranosonate

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / osmium tetroxide, N-methylmorpholine-N-oxide / 2-methyl-propan-2-ol

2: 76 percent / HCl

With hydrogenchloride; osmium(VIII) oxide; 4-methylmorpholine N-oxide; In tert-butyl alcohol;
DOI:10.1016/S0040-4039(00)78786-7