2,4,5-trichloro-6-(2,6-dibromo-4-(trifluoromethoxy)phenylamino)isophthalonitrile

Base Information

Chemical Name:2,4,5-trichloro-6-(2,6-dibromo-4-(trifluoromethoxy)phenylamino)isophthalonitrile
CAS No.:1416419-97-0
Molecular Formula:C₁₅H₃Br₂Cl₃F₃N₃O
Molecular Weight:564.371
Hs Code.:

Synonyms:2,4,5-trichloro-6-(2,6-dibromo-4-(trifluoromethoxy)phenylamino)isophthalonitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,4,5-trichloro-6-(2,6-dibromo-4-(trifluoromethoxy)phenylamino)isophthalonitrile

Chemical Property:

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Technology Process of 2,4,5-trichloro-6-(2,6-dibromo-4-(trifluoromethoxy)phenylamino)isophthalonitrile

There total 4 articles about 2,4,5-trichloro-6-(2,6-dibromo-4-(trifluoromethoxy)phenylamino)isophthalonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1416419-49-2
2,4,5-trichloro-6-(4-(trifluoromethoxy)phenylamino)isophthalonitrile

: 1416419-97-0
2,4,5-trichloro-6-(2,6-dibromo-4-(trifluoromethoxy)phenylamino)isophthalonitrile

Guidance literature:: With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; for 5h; Reflux;
DOI:10.1016/j.jfluchem.2014.01.006

Reference yield:

: 88149-49-9
2,6-dibromo-4-(trifluoromethoxy)aniline

: 1897-45-6
chlorothalonil

: 1416419-97-0
2,4,5-trichloro-6-(2,6-dibromo-4-(trifluoromethoxy)phenylamino)isophthalonitrile

Guidance literature:: With sodium hydroxide; In N,N-dimethyl-formamide; at 20 ℃; for 5h;
DOI:10.1021/jf403739e

Reference yield:

: 1897-45-6
chlorothalonil

: 461-82-5
4-(trifluoromethoxy)aniline

: 1416419-97-0
2,4,5-trichloro-6-(2,6-dibromo-4-(trifluoromethoxy)phenylamino)isophthalonitrile

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / N,N-dimethyl-formamide / 0.17 h

1.2: 2 h / 60 °C

2.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 5 h / Reflux

With N-Bromosuccinimide; sodium hydroxide; dibenzoyl peroxide; In tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.jfluchem.2014.01.006