O-[bis(benzyloxy)phosphoryl]-N-[(9H-fluoren-9-ylmethoxy)carbonyl]-D-tyrosine

Base Information

Chemical Name:O-[bis(benzyloxy)phosphoryl]-N-[(9H-fluoren-9-ylmethoxy)carbonyl]-D-tyrosine
CAS No.:1268157-63-6
Molecular Formula:C₃₈H₃₄NO₈P
Molecular Weight:663.664
Hs Code.:

Synonyms:O-[bis(benzyloxy)phosphoryl]-N-[(9H-fluoren-9-ylmethoxy)carbonyl]-D-tyrosine

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Chemical Property of O-[bis(benzyloxy)phosphoryl]-N-[(9H-fluoren-9-ylmethoxy)carbonyl]-D-tyrosine

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Technology Process of O-[bis(benzyloxy)phosphoryl]-N-[(9H-fluoren-9-ylmethoxy)carbonyl]-D-tyrosine

There total 4 articles about O-[bis(benzyloxy)phosphoryl]-N-[(9H-fluoren-9-ylmethoxy)carbonyl]-D-tyrosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₄H₄₈NO₈PSi

: 1268157-63-6
O-[bis(benzyloxy)phosphoryl]-N-[(9H-fluoren-9-ylmethoxy)carbonyl]-D-tyrosine

Guidance literature:: With water; acetic acid; In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.1021/jm101478n

Reference yield:

: C₄₄H₄₈NO₇PSi

: 1268157-63-6
O-[bis(benzyloxy)phosphoryl]-N-[(9H-fluoren-9-ylmethoxy)carbonyl]-D-tyrosine

Guidance literature:: Multi-step reaction with 2 steps

1: tert.-butylhydroperoxide / water; acetonitrile / 0.17 h / 20 °C

2: water; acetic acid / tetrahydrofuran / 1 h / 20 °C

With tert.-butylhydroperoxide; water; acetic acid; In tetrahydrofuran; water; acetonitrile;
DOI:10.1021/jm101478n

Reference yield:

: C₃₀H₃₅NO₅Si

: 1268157-63-6
O-[bis(benzyloxy)phosphoryl]-N-[(9H-fluoren-9-ylmethoxy)carbonyl]-D-tyrosine

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-tetrazole / acetonitrile / 3 h / 20 °C

2: tert.-butylhydroperoxide / water; acetonitrile / 0.17 h / 20 °C

3: water; acetic acid / tetrahydrofuran / 1 h / 20 °C

With 1H-tetrazole; tert.-butylhydroperoxide; water; acetic acid; In tetrahydrofuran; water; acetonitrile;
DOI:10.1021/jm101478n