2,5-dimethoxyphenyl acetamidyl thioether

Base Information

• Chemical Name: 2,5-dimethoxyphenyl acetamidyl thioether
• CAS No.: 1255188-07-8
• Molecular Formula: C₁₀H₁₃NO₃S
• Molecular Weight: 227.284

Synonyms:2,5-dimethoxyphenyl acetamidyl thioether

Chemical Property of 2,5-dimethoxyphenyl acetamidyl thioether

Chemical Property:

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Technology Process of 2,5-dimethoxyphenyl acetamidyl thioether

There total 1 articles about 2,5-dimethoxyphenyl acetamidyl thioether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

2,6-dimethoxybenzenethiol (26163-11-1) + Chloroacetamide (79-07-2) → 2,5-dimethoxyphenyl acetamidyl thioether (1255188-07-8)

Guidance literature:

2,6-dimethoxybenzenethiol; With sodium; In ethanol; for 0.5h; Reflux;

Chloroacetamide; With potassium iodide; In ethanol; for 5h;

DOI:10.1016/j.bmc.2010.08.002

Reference yield: 93.0%

2,5-dimethoxyphenyl acetamidyl thioether (1255188-07-8) → 2-(2,6-dimethoxyphenylthio)ethanamine (1255188-13-6)

Guidance literature:

2,5-dimethoxyphenyl acetamidyl thioether; With dimethylsulfide borane complex; In tetrahydrofuran; at 20 ℃; Inert atmosphere; Reflux;

With hydrogenchloride; In tetrahydrofuran; water; at 60 ℃; for 1h;

With sodium hydroxide; In water;

DOI:10.1016/j.bmc.2010.08.002

Reference yield: 78.0%

2,5-dimethoxyphenyl acetamidyl thioether (1255188-07-8) → 2,5-dimethoxyphenyl acetamidyl sulfoxide

Guidance literature:

With sodium periodate; In water; acetone; at 20 ℃; for 20h; Reagent/catalyst; Solvent;

DOI:10.1002/anie.201209021

upstream raw materials:

2,6-dimethoxybenzenethiol

Chloroacetamide

Downstream raw materials:

2-(2,6-dimethoxyphenylthio)ethanamine

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