C₃₅H₄₉N₃O₇

Base Information

• Chemical Name: C₃₅H₄₉N₃O₇
• CAS No.: 1009094-68-1
• Molecular Formula: C₃₅H₄₉N₃O₇
• Molecular Weight: 623.79
• Mol file: 1009094-68-1.mol

Synonyms:C₃₅H₄₉N₃O₇

Chemical Property of C₃₅H₄₉N₃O₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₅H₄₉N₃O₇

There total 9 articles about C₃₅H₄₉N₃O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + C33H45N3O7 (1009094-67-0) → C35H49N3O7 (1009094-68-1)

Guidance literature:

With sodium cyanoborohydride; acetic acid; In methanol; water; at 20 ℃;

Reference yield:

C9H10BrNO2 → C35H49N3O7 (1009094-68-1)

Guidance literature:

Multi-step reaction with 7 steps

1.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 16 h / pH 2

1.2: pH 7 / Alkaline aqueous solution

2.1: benzene / Heating / reflux

3.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation

3.2: 1 h

4.1: pyridine hydrogenfluoride / tetrahydrofuran / 3 h / 20 °C

5.1: trimethylaluminum / hexanes; dichloromethane / 0.25 h / 20 °C

5.2: 16 h / 20 °C

5.3: 2 h / 20 °C

6.1: potassium acetate; caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 4.5 h / 60 °C

7.1: sodium cyanoborohydride; acetic acid / methanol; water / 20 °C

With titanium(IV) isopropylate; hydrogenchloride; methyl orange; trimethylaluminum; potassium acetate; sodium cyanoborohydride; caesium carbonate; pyridine hydrogenfluoride; acetic acid; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; methanol; hexanes; dichloromethane; water; dimethyl sulfoxide; toluene; benzene;

Reference yield:

C9H12BrNO2 (1009091-83-1) → C35H49N3O7 (1009094-68-1)

Guidance literature:

Multi-step reaction with 6 steps

1.1: benzene / Heating / reflux

2.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation

2.2: 1 h

3.1: pyridine hydrogenfluoride / tetrahydrofuran / 3 h / 20 °C

4.1: trimethylaluminum / hexanes; dichloromethane / 0.25 h / 20 °C

4.2: 16 h / 20 °C

4.3: 2 h / 20 °C

5.1: potassium acetate; caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 4.5 h / 60 °C

6.1: sodium cyanoborohydride; acetic acid / methanol; water / 20 °C

With titanium(IV) isopropylate; trimethylaluminum; potassium acetate; sodium cyanoborohydride; caesium carbonate; pyridine hydrogenfluoride; acetic acid; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; methanol; hexanes; dichloromethane; water; dimethyl sulfoxide; toluene; benzene;

upstream raw materials:

formaldehyd

C₃₃H₄₅N₃O₇

C₉H₁₂BrNO₂

C₁₂H₁₄BrNO₄

Downstream raw materials:

C₄₆H₆₅N₅O₆

C₄₃H₆₇N₅O₆

C₄₁H₆₃N₅O₈S

C₄₈H₆₇N₅O₆