5-(benzyloxycarbonyl-O-benzyl-L-tyrosyl)aminovaleryl-L-phenylalanyl-L-leucine benzyl ester

Base Information

Chemical Name:5-(benzyloxycarbonyl-O-benzyl-L-tyrosyl)aminovaleryl-L-phenylalanyl-L-leucine benzyl ester
CAS No.:80977-32-8
Molecular Formula:C₅₁H₅₈N₄O₈
Molecular Weight:855.044
Hs Code.:

Synonyms:5-(benzyloxycarbonyl-O-benzyl-L-tyrosyl)aminovaleryl-L-phenylalanyl-L-leucine benzyl ester

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Chemical Property of 5-(benzyloxycarbonyl-O-benzyl-L-tyrosyl)aminovaleryl-L-phenylalanyl-L-leucine benzyl ester

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Technology Process of 5-(benzyloxycarbonyl-O-benzyl-L-tyrosyl)aminovaleryl-L-phenylalanyl-L-leucine benzyl ester

There total 6 articles about 5-(benzyloxycarbonyl-O-benzyl-L-tyrosyl)aminovaleryl-L-phenylalanyl-L-leucine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 73994-87-3
(S)-benzyl 2-((S)-2-amino-3-phenylpropanamido)-4-methylpentanoate hydrochloride

: 80977-31-7
5-(benzyloxycarbonyl-O-benzyl-L-tyrosyl)aminovaleric acid p-nitriphenyl ester

: 80977-32-8
5-(benzyloxycarbonyl-O-benzyl-L-tyrosyl)aminovaleryl-L-phenylalanyl-L-leucine benzyl ester

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1071/CH9812439

Reference yield:

: 73994-87-3
(S)-benzyl 2-((S)-2-amino-3-phenylpropanamido)-4-methylpentanoate hydrochloride

: 80977-28-2
5-(benzyloxycarbonyl-O-benzyl-L-tyrosyl)aminovaleric acid

: 80977-32-8
5-(benzyloxycarbonyl-O-benzyl-L-tyrosyl)aminovaleryl-L-phenylalanyl-L-leucine benzyl ester

Guidance literature:: With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In acetonitrile; at 0 ℃;
DOI:10.1071/CH9812439

Reference yield:

: 3562-03-6
Z-Tyr(OBzl)-ONp

: 80977-32-8
5-(benzyloxycarbonyl-O-benzyl-L-tyrosyl)aminovaleryl-L-phenylalanyl-L-leucine benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / N-methylmorpholine / dimethylformamide

2: 91 percent / CF₃COOH, anisole

3: 74 percent / pyridine / 48 h / Ambient temperature

4: 85 percent / Et₃N / dimethylformamide / Ambient temperature

With 4-methyl-morpholine; pyridine; methoxybenzene; triethylamine; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1071/CH9812439