methyl 1-(2'-deoxy-3',5'-di-O-p-toluoyl-α-D-erythropentofuranosyl)-4,5-imidazoledicarboxylate

Base Information

Chemical Name:methyl 1-(2'-deoxy-3',5'-di-O-p-toluoyl-α-D-erythropentofuranosyl)-4,5-imidazoledicarboxylate
CAS No.:441052-40-0
Molecular Formula:C₂₈H₂₈N₂O₉
Molecular Weight:536.538
Hs Code.:

Synonyms:methyl 1-(2'-deoxy-3',5'-di-O-p-toluoyl-α-D-erythropentofuranosyl)-4,5-imidazoledicarboxylate

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Chemical Property of methyl 1-(2'-deoxy-3',5'-di-O-p-toluoyl-α-D-erythropentofuranosyl)-4,5-imidazoledicarboxylate

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Technology Process of methyl 1-(2'-deoxy-3',5'-di-O-p-toluoyl-α-D-erythropentofuranosyl)-4,5-imidazoledicarboxylate

There total 2 articles about methyl 1-(2'-deoxy-3',5'-di-O-p-toluoyl-α-D-erythropentofuranosyl)-4,5-imidazoledicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 3304-70-9
dimethyl imidazole-4,5-dicarboxylate

: methyl 2-deoxy-3,5-di-O-p-toluoyl-β-D-erythropentofuranoside

: 441052-40-0
methyl 1-(2'-deoxy-3',5'-di-O-p-toluoyl-α-D-erythropentofuranosyl)-4,5-imidazoledicarboxylate

Guidance literature:: With chloro-trimethyl-silane; trifluorormethanesulfonic acid; 1,1,1,3,3,3-hexamethyl-disilazane; In acetonitrile; at 0 ℃; for 1h;
DOI:10.1021/jm030842j

Reference yield: 86.0%

: 3304-70-9
dimethyl imidazole-4,5-dicarboxylate

: 78185-65-6
1-O-methyl-2-deoxy-3,5-di-O-(p-toluoyl)-β-D-erythro-pentofuranose

: 441052-40-0
methyl 1-(2'-deoxy-3',5'-di-O-p-toluoyl-α-D-erythropentofuranosyl)-4,5-imidazoledicarboxylate

Guidance literature:: With chloro-trimethyl-silane; trifluorormethanesulfonic acid; 1,1,1,3,3,3-hexamethyl-disilazane; In acetonitrile; for 1h; cooling;
DOI:10.1128/AAC.46.5.1231-1239.2002