(3R,6S,7S)-7-((S)-2-methoxy-1-phenylethylamino)-6-methyl-1,7-diphenylheptan-3-ol

Base Information

Chemical Name:(3R,6S,7S)-7-((S)-2-methoxy-1-phenylethylamino)-6-methyl-1,7-diphenylheptan-3-ol
CAS No.:944454-10-8
Molecular Formula:C₂₉H₃₇NO₂
Molecular Weight:431.618
Hs Code.:

Synonyms:(3R,6S,7S)-7-((S)-2-methoxy-1-phenylethylamino)-6-methyl-1,7-diphenylheptan-3-ol

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Chemical Property of (3R,6S,7S)-7-((S)-2-methoxy-1-phenylethylamino)-6-methyl-1,7-diphenylheptan-3-ol

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Technology Process of (3R,6S,7S)-7-((S)-2-methoxy-1-phenylethylamino)-6-methyl-1,7-diphenylheptan-3-ol

There total 1 articles about (3R,6S,7S)-7-((S)-2-methoxy-1-phenylethylamino)-6-methyl-1,7-diphenylheptan-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₃H₁₇O^(1-)*Li⁽¹⁺⁾

: 153924-61-9
((S)-2-Methoxy-1-phenyl-ethyl)-[1-phenyl-meth-(E)-ylidene]-amine

: 944454-10-8
(3R,6S,7S)-7-((S)-2-methoxy-1-phenylethylamino)-6-methyl-1,7-diphenylheptan-3-ol

: (3R,7S)-7-((S)-2-methoxy-1-phenylethylamino)-6-methyl-1,7-diphenylheptan-3-ol

Guidance literature:: ((S)-2-Methoxy-1-phenyl-ethyl)-[1-phenyl-meth-(E)-ylidene]-amine; With titanium(IV) isopropylate; cyclopentylmagnesium chloride; In diethyl ether; at -60 - -30 ℃; for 2.5h;

C₁₃H₁₇O^(1-)*Li⁽¹⁺⁾; In diethyl ether; hexane; at -30 - 20 ℃; for 6.5h; Further stages.;
DOI:10.1021/ja071974v

Reference yield: 92.0%

: 944454-10-8
(3R,6S,7S)-7-((S)-2-methoxy-1-phenylethylamino)-6-methyl-1,7-diphenylheptan-3-ol

: 944454-19-7
(3R,6S,7S)-7-amino-6-methyl-1,7-diphenylheptan-3-ol

Guidance literature:: With hydrogen; acetic acid; palladium dihydroxide; In methanol; water; at 20 ℃; for 6h; under 760.051 Torr;
DOI:10.1021/ja071974v

Reference yield:

: 944454-10-8
(3R,6S,7S)-7-((S)-2-methoxy-1-phenylethylamino)-6-methyl-1,7-diphenylheptan-3-ol

: 944454-22-2
N-((1S,2S,5R)-5-hydroxy-2-methyl-1,7-diphenylheptyl)-2-nitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / H₂; AcOH / Pd(OH)2 / methanol; H₂O / 6 h / 20 °C / 760.05 Torr

2: 91 percent / Et₃N; 4-(dimethylamino)pyridine / CH₂Cl₂ / 2.25 h / 0 - 20 °C

With dmap; hydrogen; acetic acid; triethylamine; palladium dihydroxide; In methanol; dichloromethane; water;
DOI:10.1021/ja071974v