2-methyl-1-phenylsulfonylcyclopentene

Base Information

• Chemical Name: 2-methyl-1-phenylsulfonylcyclopentene
• CAS No.: 96530-14-2
• Molecular Formula: C₁₂H₁₄O₂S
• Molecular Weight: 222.308
• Mol file: 96530-14-2.mol

Synonyms:2-methyl-1-phenylsulfonylcyclopentene

Chemical Property of 2-methyl-1-phenylsulfonylcyclopentene

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 2-methyl-1-phenylsulfonylcyclopentene

There total 14 articles about 2-methyl-1-phenylsulfonylcyclopentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

6-iodo-3-(phenylsulfonyl)hexa-1,2-diene (136339-10-1) → 2-methyl-1-phenylsulfonylcyclopentene (96530-14-2)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 2h; Heating;

DOI:10.1016/S0040-4039(00)79759-0

Reference yield: 24.1%

1-(phenylthio)-2-methylcyclopentene (67957-90-8) → 2-methyl-1-phenylsulfinylcyclopentene (96530-15-3) + 2-methyl-1-phenylsulfonylcyclopentene (96530-14-2)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In chloroform; for 0.75h;

Reference yield:

(1-Benzenesulfonyl-2-methyl-cyclopent-2-enyl)-trimethyl-silane (150583-32-7) → 2-methyl-1-phenylsulfonylcyclopentene (96530-14-2)

Guidance literature:

With toluene-4-sulfonic acid; In benzene; at 70 ℃; for 12h; Yield given;

DOI:10.1016/S0040-4039(00)60467-7

upstream raw materials:

1-(phenylthio)-2-methylcyclopentene

6-iodo-3-(phenylsulfonyl)hexa-1,2-diene

(1-Benzenesulfonyl-2-methyl-cyclopent-2-enyl)-trimethyl-silane

5-bromo-1-methyl-cyclopentene