Technology Process of C54H66FN5O10Si2
There total 8 articles about C54H66FN5O10Si2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C53H62FN5O10Si2;
With
sodium cyanoborohydride; acetic acid;
at 5 - 20 ℃;
for 1.25h;
formaldehyd;
With
sodium cyanoborohydride;
In
water;
at 5 - 20 ℃;
for 1.25h;
DOI:10.1081/NCN-120028337
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 89 percent / imidazole / dimethylformamide / 12 h / 20 °C
2.1: 95 percent / methylhydrazine / CH2Cl2 / 1 h / 0 °C
3.1: acetic acid / CH2Cl2; toluene / 35 °C / atmospheric pressure
4.1: sodium cyanoborohydride; glacial acetic acid / 1.25 h / 5 - 20 °C
4.2: 2.80 g / sodium cyanoborohydride / H2O / 1.25 h / 5 - 20 °C
With
1H-imidazole; sodium cyanoborohydride; acetic acid; methylhydrazine;
In
dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1081/NCN-120028337
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium; hexamethylphosphoramide / tetrahydrofuran; pentane / 1 h / -78 °C
1.2: 69 percent / hexamethylphosphoramide / tetrahydrofuran; pentane / 1.5 h
2.1: 55 percent / mercuric chloride; mercuric oxide; H2O / tetrahydrofuran / 0.25 h / -5 °C
3.1: acetic acid / CH2Cl2; toluene / 35 °C / atmospheric pressure
4.1: sodium cyanoborohydride; glacial acetic acid / 1.25 h / 5 - 20 °C
4.2: 2.80 g / sodium cyanoborohydride / H2O / 1.25 h / 5 - 20 °C
With
N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; water; sodium cyanoborohydride; acetic acid; mercury dichloride; mercury(II) oxide;
In
tetrahydrofuran; dichloromethane; toluene; pentane;
DOI:10.1081/NCN-120028337
