N-cinnamyl-2α-(o-bromophenyl)-4,4,7α-trimethyl-trans-octahydro-1,3-benzoxazine

Base Information

Chemical Name:N-cinnamyl-2α-(o-bromophenyl)-4,4,7α-trimethyl-trans-octahydro-1,3-benzoxazine
CAS No.:334706-52-4
Molecular Formula:C₂₆H₃₂BrNO
Molecular Weight:454.45
Hs Code.:

Synonyms:N-cinnamyl-2α-(o-bromophenyl)-4,4,7α-trimethyl-trans-octahydro-1,3-benzoxazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-cinnamyl-2α-(o-bromophenyl)-4,4,7α-trimethyl-trans-octahydro-1,3-benzoxazine

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Technology Process of N-cinnamyl-2α-(o-bromophenyl)-4,4,7α-trimethyl-trans-octahydro-1,3-benzoxazine

There total 2 articles about N-cinnamyl-2α-(o-bromophenyl)-4,4,7α-trimethyl-trans-octahydro-1,3-benzoxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 4392-24-9
3-bromo-1-phenyl-1-propenyl bromide

: 334706-50-2
2α-(o-bromophenyl)-4,4,7α-trimethyl-trans-octahydro-1,3-benzoxazine

: 334706-52-4
N-cinnamyl-2α-(o-bromophenyl)-4,4,7α-trimethyl-trans-octahydro-1,3-benzoxazine

Guidance literature:: With potassium carbonate; In acetonitrile; Heating;
DOI:10.1016/S0040-4020(01)00274-5

Reference yield:

: 55179-51-6
(-)-aminomenthol

: 334706-52-4
N-cinnamyl-2α-(o-bromophenyl)-4,4,7α-trimethyl-trans-octahydro-1,3-benzoxazine

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / CH₂Cl₂ / 4 h / 20 °C

2: 91 percent / potassium carbonate / acetonitrile / Heating

With potassium carbonate; In dichloromethane; acetonitrile;
DOI:10.1016/S0040-4020(01)00274-5

Reference yield: 43.0%

: 334706-52-4
N-cinnamyl-2α-(o-bromophenyl)-4,4,7α-trimethyl-trans-octahydro-1,3-benzoxazine

: 350508-53-1
(2S,4aS,7R,8aR)-4,4,7-trimethyl-2-phenyl-octahydro-benz[e][1,3]oxazine

: 334706-84-2
(5R,7aS,10R,11aR,12aS)-5-Benzyl-7,7,10-trimethyl-5,7a,8,9,10,11,11a,12a-octahydro-6H,7H-12-oxa-6a-aza-benzo[a]anthracene

: (5S,7aS,10R,11aR,12aS)-5-Benzyl-7,7,10-trimethyl-5,7a,8,9,10,11,11a,12a-octahydro-6H,7H-12-oxa-6a-aza-benzo[a]anthracene

Guidance literature:: N-cinnamyl-2α-(o-bromophenyl)-4,4,7α-trimethyl-trans-octahydro-1,3-benzoxazine; With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 44h; Heating;

With potassium fluoride; In diethyl ether; water; at 20 ℃; for 4h;

With silica gel; In hexane; ethyl acetate;
DOI:10.1016/S0040-4020(01)00274-5