dithiocarbonic acid O-ethyl ester S-(2-iodo-5-methoxyphenyl)

Base Information

• Chemical Name: dithiocarbonic acid O-ethyl ester S-(2-iodo-5-methoxyphenyl)
• CAS No.: 874903-81-8
• Molecular Formula: C₁₀H₁₁IO₂S₂
• Molecular Weight: 354.233
• Mol file: 874903-81-8.mol

Synonyms:dithiocarbonic acid O-ethyl ester S-(2-iodo-5-methoxyphenyl)

Chemical Property of dithiocarbonic acid O-ethyl ester S-(2-iodo-5-methoxyphenyl)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of dithiocarbonic acid O-ethyl ester S-(2-iodo-5-methoxyphenyl)

There total 2 articles about dithiocarbonic acid O-ethyl ester S-(2-iodo-5-methoxyphenyl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

potassium ethyl xanthogenate (140-89-6) + 2-iodo-5-methoxybenzenediazonium tetrafluoroborate → dithiocarbonic acid O-ethyl ester S-(2-iodo-5-methoxyphenyl) (874903-81-8)

Guidance literature:

In acetone; at -20 - 20 ℃;

DOI:10.1021/jm0503087

Reference yield:

2-iodo-5-methoxyaniline (153898-63-6) → dithiocarbonic acid O-ethyl ester S-(2-iodo-5-methoxyphenyl) (874903-81-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 94 percent / HBF₄; NaNO₂ / H₂O / 0.5 h / 0 - 20 °C

2: acetone / 1.75 h / 0 - 20 °C

With tetrafluoroboric acid; sodium nitrite; In water; acetone;

DOI:10.1021/ol0067179

Reference yield:

dithiocarbonic acid O-ethyl ester S-(2-iodo-5-methoxyphenyl) (874903-81-8) → potassium; 2-iodo-5-methoxy-benzenethiolate

Guidance literature:

With potassium hydroxide; In tetrahydrofuran; methanol; at 40 ℃; for 2h;

DOI:10.1021/jm0503087

upstream raw materials:

potassium ethyl xanthogenate

2-iodo-5-methoxyaniline

Downstream raw materials:

2-[6-amino-8-(2-iodo-5-methoxy-phenylsulfanyl)purin-9-yl]ethanol

benzyl 2-iodo-5-methoxyphenyl sulfide

3-iodo-6-methoxy-2-(4-methoxyphenyl)benzo[b]thiophene

2-Benzylsulfanyl-4-methoxy-1-(4-methoxy-phenylethynyl)-benzene