8-[(4-methylpiperidin-1-yl)carbonyl]-5-(phenylsulfonyl)-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole trifluoroacetate

Base Information

Chemical Name:8-[(4-methylpiperidin-1-yl)carbonyl]-5-(phenylsulfonyl)-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole trifluoroacetate
CAS No.:910801-36-4
Molecular Formula:C₂HF₃O₂*C₂₄H₂₇N₃O₃S
Molecular Weight:551.587
Hs Code.:

Synonyms:8-[(4-methylpiperidin-1-yl)carbonyl]-5-(phenylsulfonyl)-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole trifluoroacetate

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Chemical Property of 8-[(4-methylpiperidin-1-yl)carbonyl]-5-(phenylsulfonyl)-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole trifluoroacetate

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Technology Process of 8-[(4-methylpiperidin-1-yl)carbonyl]-5-(phenylsulfonyl)-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole trifluoroacetate

There total 4 articles about 8-[(4-methylpiperidin-1-yl)carbonyl]-5-(phenylsulfonyl)-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 910801-34-2
tert-butyl 8-[(4-methylpiperidin-1-yl)carbonyl]-5-(phenylsulfonyl)-1,3,4,5-tetrahydro-2H-pyrido[4,3-b]indole-2-carboxylate

: 76-05-1
trifluoroacetic acid

: 910801-36-4
8-[(4-methylpiperidin-1-yl)carbonyl]-5-(phenylsulfonyl)-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole trifluoroacetate

Guidance literature:: In dichloromethane; at 20 ℃; for 0.5h;

Reference yield:

: 626-58-4
4-methylpiperidin

: 910801-36-4
8-[(4-methylpiperidin-1-yl)carbonyl]-5-(phenylsulfonyl)-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 1 h / 20 °C

2: potassium tert-butylate / N,N-dimethyl-formamide / 1 h / 20 °C

3: dichloromethane / 0.5 h / 20 °C

With potassium tert-butylate; N-ethyl-N,N-diisopropylamine; HATU; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 910797-04-5
tert-butyl 8-[(4-methylpiperidin-1-yl)carbonyl]-1,3,4,5-tetrahydro-2H-pyrido[4,3-b]indole-2-carboxylate

: 910801-36-4
8-[(4-methylpiperidin-1-yl)carbonyl]-5-(phenylsulfonyl)-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / N,N-dimethyl-formamide / 1 h / 20 °C

2: dichloromethane / 0.5 h / 20 °C

With potassium tert-butylate; In dichloromethane; N,N-dimethyl-formamide;