1-(4-chlorophenyl)vinyl isopropylphenylcarbamate

Base Information

Chemical Name:1-(4-chlorophenyl)vinyl isopropylphenylcarbamate
CAS No.:1350911-29-3
Molecular Formula:C₁₈H₁₈ClNO₂
Molecular Weight:315.799
Hs Code.:

Synonyms:1-(4-chlorophenyl)vinyl isopropylphenylcarbamate

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Chemical Property of 1-(4-chlorophenyl)vinyl isopropylphenylcarbamate

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Technology Process of 1-(4-chlorophenyl)vinyl isopropylphenylcarbamate

There total 2 articles about 1-(4-chlorophenyl)vinyl isopropylphenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 40016-69-1
N-isopropyl-N-phenyl-carbamoyl chloride

: 99-91-2
para-chloroacetophenone

: 1350911-29-3
1-(4-chlorophenyl)vinyl isopropylphenylcarbamate

Guidance literature:: With sodium methylsulfinylmethanide; In dimethyl sulfoxide; at 20 ℃; for 15h; Inert atmosphere;
DOI:10.1021/ol2029355

Reference yield:

: 768-52-5
N-Isopropylaniline

: 1350911-29-3
1-(4-chlorophenyl)vinyl isopropylphenylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 2 h / 20 °C / Inert atmosphere

2: sodium methylsulfinylmethanide / dimethyl sulfoxide / 15 h / 20 °C / Inert atmosphere

With pyridine; sodium methylsulfinylmethanide; In dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ol2029355

Reference yield: 55.0%

: 109-72-8,29786-93-4
n-butyllithium

: 1350911-29-3
1-(4-chlorophenyl)vinyl isopropylphenylcarbamate

: 1350911-69-1
1-(4-chlorophenyl)-1-phenylhexan-1-ol

Guidance literature:: n-butyllithium; 1-(4-chlorophenyl)vinyl isopropylphenylcarbamate; In tetrahydrofuran; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; hexane; at -78 ℃; for 0.25h; Inert atmosphere;

With tert.-butylnitrite; In tetrahydrofuran; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; hexane; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ol2029355