1,4-(diacetylseleno)benzene

Base Information

Chemical Name:1,4-(diacetylseleno)benzene
CAS No.:529514-59-8
Molecular Formula:C₁₀H₁₀O₂Se₂
Molecular Weight:320.108
Hs Code.:

Synonyms:1,4-(diacetylseleno)benzene

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Chemical Property of 1,4-(diacetylseleno)benzene

Chemical Property:

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Technology Process of 1,4-(diacetylseleno)benzene

There total 1 articles about 1,4-(diacetylseleno)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 106-37-6
1.4-dibromobenzene

: 75-36-5
acetyl chloride

: 529514-59-8
1,4-(diacetylseleno)benzene

Guidance literature:: 1.4-dibromobenzene; With tert.-butyl lithium; In tetrahydrofuran; pentane; at -78 - 0 ℃; for 2.5h; Inert atmosphere; Schlenk technique;

With selenium; In tetrahydrofuran; pentane; at 0 ℃; for 0.5h; Inert atmosphere; Schlenk technique;

acetyl chloride; In tetrahydrofuran; pentane; at -78 - 20 ℃; for 14h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c7tc03277c

Reference yield:

: 529514-59-8
1,4-(diacetylseleno)benzene

: 36987-10-7
benzene-1,4-diselenol

Guidance literature:: With ethanol; toluene-4-sulfonic acid; In toluene; at 80 ℃; for 8h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c7tc03277c

Reference yield:

: 529514-59-8
1,4-(diacetylseleno)benzene

: C₆H₄Se₂^(2-)*C₆H₅Bi⁽²⁺⁾

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid; ethanol / toluene / 8 h / 80 °C / Inert atmosphere; Schlenk technique

2: toluene / 72 h / 25 °C / Inert atmosphere; Schlenk technique

With ethanol; toluene-4-sulfonic acid; In toluene;
DOI:10.1039/c7tc03277c