ethyl 2-(2-chloro-5-((2S)-3-(5-chloro-1'H,3H-spiro[1-benzofuran-2,4'-piperidin]-1'-yl)-2-hydroxypropyloxy)-4-methylaminocarbonylphenoxy)-2-methylpropanoate trifluoroacetate

Base Information

Chemical Name:ethyl 2-(2-chloro-5-((2S)-3-(5-chloro-1'H,3H-spiro[1-benzofuran-2,4'-piperidin]-1'-yl)-2-hydroxypropyloxy)-4-methylaminocarbonylphenoxy)-2-methylpropanoate trifluoroacetate
CAS No.:1003567-29-0
Molecular Formula:C₂HF₃O₂*C₂₉H₃₆Cl₂N₂O₇
Molecular Weight:709.544
Hs Code.:

ethyl 2-(2-chloro-5-((2S)-3-(5-chloro-1'H,3H-spiro[1-benzofuran-2,4'-piperidin]-1'-yl)-2-hydroxypropyloxy)-4-methylaminocarbonylphenoxy)-2-methylpropanoate trifluoroacetate

Synonyms:ethyl 2-(2-chloro-5-((2S)-3-(5-chloro-1'H,3H-spiro[1-benzofuran-2,4'-piperidin]-1'-yl)-2-hydroxypropyloxy)-4-methylaminocarbonylphenoxy)-2-methylpropanoate trifluoroacetate

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Chemical Property of ethyl 2-(2-chloro-5-((2S)-3-(5-chloro-1'H,3H-spiro[1-benzofuran-2,4'-piperidin]-1'-yl)-2-hydroxypropyloxy)-4-methylaminocarbonylphenoxy)-2-methylpropanoate trifluoroacetate

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Technology Process of ethyl 2-(2-chloro-5-((2S)-3-(5-chloro-1'H,3H-spiro[1-benzofuran-2,4'-piperidin]-1'-yl)-2-hydroxypropyloxy)-4-methylaminocarbonylphenoxy)-2-methylpropanoate trifluoroacetate

There total 2 articles about ethyl 2-(2-chloro-5-((2S)-3-(5-chloro-1'H,3H-spiro[1-benzofuran-2,4'-piperidin]-1'-yl)-2-hydroxypropyloxy)-4-methylaminocarbonylphenoxy)-2-methylpropanoate trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 600-00-0
ethyl 2-bromoisobutyrate

: 1003567-13-2
5-chloro-2-{[(2S)-3-(5-chloro-3H-spiro[1-benzofuran-2,4'-piperidin]-1'-yl)-2-hydroxypropyl]oxy}-4-hydroxy-N-methylbenzamide trifluoroacetic acid salt

: 1003567-29-0
ethyl 2-(2-chloro-5-((2S)-3-(5-chloro-1'H,3H-spiro[1-benzofuran-2,4'-piperidin]-1'-yl)-2-hydroxypropyloxy)-4-methylaminocarbonylphenoxy)-2-methylpropanoate trifluoroacetate

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 45 ℃;

Reference yield: 86.0%

: 600-00-0
ethyl 2-bromoisobutyrate

: 1003567-13-2
5-chloro-2-{[(2S)-3-(5-chloro-3H-spiro[1-benzofuran-2,4'-piperidin]-1'-yl)-2-hydroxypropyl]oxy}-4-hydroxy-N-methylbenzamide trifluoroacetic acid salt

: 76-05-1
trifluoroacetic acid

: 1003567-29-0
ethyl 2-(2-chloro-5-((2S)-3-(5-chloro-1'H,3H-spiro[1-benzofuran-2,4'-piperidin]-1'-yl)-2-hydroxypropyloxy)-4-methylaminocarbonylphenoxy)-2-methylpropanoate trifluoroacetate

Guidance literature:: ethyl 2-bromoisobutyrate; 5-chloro-2-{[(2S)-3-(5-chloro-3H-spiro[1-benzofuran-2,4'-piperidin]-1'-yl)-2-hydroxypropyl]oxy}-4-hydroxy-N-methylbenzamide trifluoroacetic acid salt; With caesium carbonate; In N,N-dimethyl-formamide; at 45 ℃;

trifluoroacetic acid;

Reference yield: 45.0%

: 1003567-29-0
ethyl 2-(2-chloro-5-((2S)-3-(5-chloro-1'H,3H-spiro[1-benzofuran-2,4'-piperidin]-1'-yl)-2-hydroxypropyloxy)-4-methylaminocarbonylphenoxy)-2-methylpropanoate trifluoroacetate

: 76-05-1
trifluoroacetic acid

: 2-(2-chloro-5-((2S)-3-(5-chloro-1'H,3H-spiro[1-benzofuran-2,4'-piperidin]-1'-yl)-2-hydroxypropyloxy)-4-methylaminocarbonylphenoxy)-2-methylpropanoic acid trifluoroacetate

Guidance literature:: ethyl 2-(2-chloro-5-((2S)-3-(5-chloro-1'H,3H-spiro[1-benzofuran-2,4'-piperidin]-1'-yl)-2-hydroxypropyloxy)-4-methylaminocarbonylphenoxy)-2-methylpropanoate trifluoroacetate; With sodium hydroxide; water; In 1,4-dioxane; at 80 ℃; for 0.5h;

With hydrogenchloride; In 1,4-dioxane; water;

trifluoroacetic acid;