1L-2,4,5,7-Tetra-O-benzyl-1-desoxy-1-C-(hydroxymethyl)-3-O-<(2-methoxyethoxy)methyl>-6-O-methyl-myo-inosit

Base Information

Chemical Name:1L-2,4,5,7-Tetra-O-benzyl-1-desoxy-1-C-(hydroxymethyl)-3-O-<(2-methoxyethoxy)methyl>-6-O-methyl-myo-inosit
CAS No.:97119-70-5
Molecular Formula:C₄₀H₄₈O₈
Molecular Weight:664.753
Hs Code.:

1L-2,4,5,7-Tetra-O-<D2>benzyl-1-desoxy-1-C-(hydroxymethyl)-3-O-<(2-methoxyethoxy)methyl>-6-O-methyl-myo-inosit

Synonyms:1L-2,4,5,7-Tetra-O-benzyl-1-desoxy-1-C-(hydroxymethyl)-3-O-<(2-methoxyethoxy)methyl>-6-O-methyl-myo-inosit

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Chemical Property of 1L-2,4,5,7-Tetra-O-benzyl-1-desoxy-1-C-(hydroxymethyl)-3-O-<(2-methoxyethoxy)methyl>-6-O-methyl-myo-inosit

Chemical Property:

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Technology Process of 1L-2,4,5,7-Tetra-O-benzyl-1-desoxy-1-C-(hydroxymethyl)-3-O-<(2-methoxyethoxy)methyl>-6-O-methyl-myo-inosit

There total 12 articles about 1L-2,4,5,7-Tetra-O-benzyl-1-desoxy-1-C-(hydroxymethyl)-3-O-<(2-methoxyethoxy)methyl>-6-O-methyl-myo-inosit which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 51271-29-5
[1',1'-2H₂]benzyl bromide

: 97119-69-2
1L-4,5,7-Tri-O-benzyl-1-desoxy-1-C-(hydroxymethyl)-3-O-<(2-methoxyethoxy)methyl>-6-O-methyl-myo-inosit

: 97119-70-5
1L-2,4,5,7-Tetra-O-benzyl-1-desoxy-1-C-(hydroxymethyl)-3-O-<(2-methoxyethoxy)methyl>-6-O-methyl-myo-inosit

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; 1) 2 h, 0 deg C, 2) 5 h, room temp.;

Reference yield:

: 51271-29-5
[1',1'-2H₂]benzyl bromide

: 97119-70-5
1L-2,4,5,7-Tetra-O-benzyl-1-desoxy-1-C-(hydroxymethyl)-3-O-<(2-methoxyethoxy)methyl>-6-O-methyl-myo-inosit

Guidance literature:: Multi-step reaction with 9 steps

1: 94 percent / 1) NaH / dimethylformamide / 1) 2 h, 0 deg C, 2) 5 h, room temp.

2: 81 percent / 98percent acetic acid / 30 °C

3: 91 percent / 1) NaH / dimethylformamide / 1) 2 h, 0 deg C, 2) 5 h, room temp.

4: 91 percent / acetic acid / tetrahydrofuran; H₂O / 60 °C

5: p-toluenesulfonic acid / toluene / 0.17 h / Ambient temperature

6: 90percent acetic acid / toluene / 0.08 h

7: 89 percent / ethyldiisopropylamine / CH₂Cl₂

8: 1 N NaOCH₃ / methanol

9: 91 percent / 1) NaH / dimethylformamide / 1) 2 h, 0 deg C, 2) 5 h, room temp.

With sodium methylate; sodium hydride; toluene-4-sulfonic acid; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 86845-47-8,86853-27-2
1L-1-Desoxy-1-C-hydroxymethyl-2,3:4,5-di-O-isopropyliden-6-O-methyl-myo-inosit

: 97119-70-5
1L-2,4,5,7-Tetra-O-benzyl-1-desoxy-1-C-(hydroxymethyl)-3-O-<(2-methoxyethoxy)methyl>-6-O-methyl-myo-inosit

Guidance literature:: Multi-step reaction with 9 steps

1: 94 percent / 1) NaH / dimethylformamide / 1) 2 h, 0 deg C, 2) 5 h, room temp.

2: 81 percent / 98percent acetic acid / 30 °C

3: 91 percent / 1) NaH / dimethylformamide / 1) 2 h, 0 deg C, 2) 5 h, room temp.

4: 91 percent / acetic acid / tetrahydrofuran; H₂O / 60 °C

5: p-toluenesulfonic acid / toluene / 0.17 h / Ambient temperature

6: 90percent acetic acid / toluene / 0.08 h

7: 89 percent / ethyldiisopropylamine / CH₂Cl₂

8: 1 N NaOCH₃ / methanol

9: 91 percent / 1) NaH / dimethylformamide / 1) 2 h, 0 deg C, 2) 5 h, room temp.

With sodium methylate; sodium hydride; toluene-4-sulfonic acid; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;