N-(4-acetamido-5-methoxy-2-nitrophenyl)-N-(2-propenyl)methanesulfonamide

Base Information

Chemical Name:N-(4-acetamido-5-methoxy-2-nitrophenyl)-N-(2-propenyl)methanesulfonamide
CAS No.:116911-56-9
Molecular Formula:C₁₃H₁₇N₃O₆S
Molecular Weight:343.36
Hs Code.:

Synonyms:N-(4-acetamido-5-methoxy-2-nitrophenyl)-N-(2-propenyl)methanesulfonamide

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Chemical Property of N-(4-acetamido-5-methoxy-2-nitrophenyl)-N-(2-propenyl)methanesulfonamide

Chemical Property:

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Technology Process of N-(4-acetamido-5-methoxy-2-nitrophenyl)-N-(2-propenyl)methanesulfonamide

There total 5 articles about N-(4-acetamido-5-methoxy-2-nitrophenyl)-N-(2-propenyl)methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 116911-55-8
N-(4-acetamido-5-mthoxy-2-nitrophenyl)methanesulfonamide

: 106-95-6
allyl bromide

: 116911-56-9
N-(4-acetamido-5-methoxy-2-nitrophenyl)-N-(2-propenyl)methanesulfonamide

Guidance literature:: With potassium tert-butylate; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)84617-1

Reference yield:

: 93-27-6
5-nitro-2-acetylaminoanisole

: 116911-56-9
N-(4-acetamido-5-methoxy-2-nitrophenyl)-N-(2-propenyl)methanesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: 5percent palladium on charcoal, hydrogen / ethyl acetate / 3 h

2: 57 percent / pyridine / CHCl₃ / 2 h / 0 - 25 °C

3: 71 percent / mercuric acetate, 70percent nitric acid / acetic acid; acetic anhydride / 0.5 h / 0 °C

4: potassium tert-butoxide / dimethylformamide / 4 h / 0 - 15 °C

With pyridine; palladium on activated charcoal; potassium tert-butylate; mercury(II) diacetate; hydrogen; nitric acid; In chloroform; acetic anhydride; acetic acid; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jo00256a036

Reference yield:

: 97-52-9
2-methoxy-4-nitrophenylamine

: 116911-56-9
N-(4-acetamido-5-methoxy-2-nitrophenyl)-N-(2-propenyl)methanesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine

2: 1.) H₂ / 1.) Pd-C / 2.) pyridine

3: HNO₃, Hg(OAc)2 / acetic acid; acetic anhydride

4: KOC(CH₃)3 / dimethylformamide

With potassium tert-butylate; mercury(II) diacetate; hydrogen; nitric acid; palladium on activated charcoal; In pyridine; acetic anhydride; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)84617-1