C₆₄H₅₈O₁₃

Base Information

Chemical Name:C₆₄H₅₈O₁₃
CAS No.:148014-79-3
Molecular Formula:C₆₄H₅₈O₁₃
Molecular Weight:1035.16
Hs Code.:

C<sub>64</sub>H<sub>58</sub>O<sub>13</sub>

Synonyms:C₆₄H₅₈O₁₃

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Chemical Property of C₆₄H₅₈O₁₃

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Technology Process of C₆₄H₅₈O₁₃

There total 7 articles about C₆₄H₅₈O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-Benzyloxy-2-methoxy-3,5,6-trimethyl-benzoic acid

: 148014-79-3
C₆₄H₅₈O₁₃

Guidance literature:: Multi-step reaction with 3 steps

1: 3.8 g / H₂ / Pd/C / methanol; ethyl acetate

2: ethyl acetate / Ambient temperature

3: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, from -78 deg C, 10 min to RT, overnight

With n-butyllithium; hydrogen; palladium on activated charcoal; In methanol; ethyl acetate;
DOI:10.1021/jm960437a

Reference yield:

: 7120-41-4
methyl 5-bromo-2-methoxybenzoate

: 148014-79-3
C₆₄H₅₈O₁₃

Guidance literature:: Multi-step reaction with 4 steps

1: 1,) NaH, 2.) CuBr*Me₂S / 1.) DMF, 1.5 h, 2.) DMF, reflux, 22 h

2: aq. KOH / methanol

3: oxalyl chloride / CH₂Cl₂ / a) RT, 30 min, b) reflux, 30 min

4: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, from -78 deg C, 10 min to RT, overnight

With potassium hydroxide; n-butyllithium; oxalyl dichloride; copper(I) bromide dimethylsulfide complex; sodium hydride; In methanol; dichloromethane;
DOI:10.1021/jm960437a

Reference yield:

: 148014-77-1
bis(3-carboxy-4-methoxyphenyl) ether

: 148014-79-3
C₆₄H₅₈O₁₃

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride / CH₂Cl₂ / a) RT, 30 min, b) reflux, 30 min

2: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, from -78 deg C, 10 min to RT, overnight

With n-butyllithium; oxalyl dichloride; In dichloromethane;
DOI:10.1021/jm960437a