2-(6-(tert-butoxycarbonylaminomethyl)benzo[d][1,3]dioxol-5-yl)-6-(ethoxycarbonylmethyl)cyclohex-2-enone

Base Information

Chemical Name:2-(6-(tert-butoxycarbonylaminomethyl)benzo[d][1,3]dioxol-5-yl)-6-(ethoxycarbonylmethyl)cyclohex-2-enone
CAS No.:1448847-26-4
Molecular Formula:C₂₃H₂₉NO₇
Molecular Weight:431.486
Hs Code.:

Synonyms:2-(6-(tert-butoxycarbonylaminomethyl)benzo[d][1,3]dioxol-5-yl)-6-(ethoxycarbonylmethyl)cyclohex-2-enone

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Chemical Property of 2-(6-(tert-butoxycarbonylaminomethyl)benzo[d][1,3]dioxol-5-yl)-6-(ethoxycarbonylmethyl)cyclohex-2-enone

Chemical Property:

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Technology Process of 2-(6-(tert-butoxycarbonylaminomethyl)benzo[d][1,3]dioxol-5-yl)-6-(ethoxycarbonylmethyl)cyclohex-2-enone

There total 3 articles about 2-(6-(tert-butoxycarbonylaminomethyl)benzo[d][1,3]dioxol-5-yl)-6-(ethoxycarbonylmethyl)cyclohex-2-enone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1448847-25-3
6-(tert-butoxycarbonylaminomethyl)benzo[d][1,3]dioxol-5-ylboronic acid

: 1426390-41-1
C₁₀H₁₃IO₃

: 1448847-26-4
2-(6-(tert-butoxycarbonylaminomethyl)benzo[d][1,3]dioxol-5-yl)-6-(ethoxycarbonylmethyl)cyclohex-2-enone

Guidance literature:: With palladium 10% on activated carbon; sodium carbonate; In 1,2-dimethoxyethane; water; at 20 ℃; for 12h;
DOI:10.1002/anie.201207561

Reference yield:

: 930-68-7
cyclohexenone

: 1448847-26-4
2-(6-(tert-butoxycarbonylaminomethyl)benzo[d][1,3]dioxol-5-yl)-6-(ethoxycarbonylmethyl)cyclohex-2-enone

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C

1.2: 2.5 h / -78 °C

2.1: iodine; potassium carbonate; dmap / water; tetrahydrofuran / 20 °C

3.1: palladium 10% on activated carbon; sodium carbonate / water; 1,2-dimethoxyethane / 12 h / 20 °C

With dmap; palladium 10% on activated carbon; iodine; sodium carbonate; potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; 1,2-dimethoxyethane; water;
DOI:10.1002/anie.201207561

Reference yield:

: 111248-50-1
ethyl 2-(2-oxocyclohex-3-en-1-yl)acetate

: 1448847-26-4
2-(6-(tert-butoxycarbonylaminomethyl)benzo[d][1,3]dioxol-5-yl)-6-(ethoxycarbonylmethyl)cyclohex-2-enone

Guidance literature:: Multi-step reaction with 2 steps

1: iodine; potassium carbonate; dmap / water; tetrahydrofuran / 20 °C

2: palladium 10% on activated carbon; sodium carbonate / water; 1,2-dimethoxyethane / 12 h / 20 °C

With dmap; palladium 10% on activated carbon; iodine; sodium carbonate; potassium carbonate; In tetrahydrofuran; 1,2-dimethoxyethane; water;
DOI:10.1002/anie.201207561