(2R,3R,R_S)-(-)-2-[3-(4-methoxyphenyl)propyl]-2-(p-tolylsulfinyl)-1,3-diphenylaziridine

Base Information

• Chemical Name: (2R,3R,R_S)-(-)-2-[3-(4-methoxyphenyl)propyl]-2-(p-tolylsulfinyl)-1,3-diphenylaziridine
• CAS No.: 351388-30-2
• Molecular Formula: C₃₁H₃₁NO₂S
• Molecular Weight: 481.659

Synonyms:(2R,3R,R_S)-(-)-2-[3-(4-methoxyphenyl)propyl]-2-(p-tolylsulfinyl)-1,3-diphenylaziridine

Chemical Property of (2R,3R,R_S)-(-)-2-[3-(4-methoxyphenyl)propyl]-2-(p-tolylsulfinyl)-1,3-diphenylaziridine

Chemical Property:

Purity/Quality:

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Technology Process of (2R,3R,R_S)-(-)-2-[3-(4-methoxyphenyl)propyl]-2-(p-tolylsulfinyl)-1,3-diphenylaziridine

There total 3 articles about (2R,3R,R_S)-(-)-2-[3-(4-methoxyphenyl)propyl]-2-(p-tolylsulfinyl)-1,3-diphenylaziridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R)-chloromethyl p-tolyl sulfoxide (31350-91-1) → (2R,3R,RS)-(-)-2-[3-(4-methoxyphenyl)propyl]-2-(p-tolylsulfinyl)-1,3-diphenylaziridine (351388-30-2)

Guidance literature:

Multi-step reaction with 3 steps

1.1: lithium diisopropylamide / tetrahydrofuran / 0.17 h

1.2: 99 percent / tetrahydrofuran

2.1: lithium diisopropylamide / tetrahydrofuran / 0.17 h

2.2: 98 percent / tetrahydrofuran / 0.17 h

3.1: 79 percent / potassium tert-butoxide / 2-methyl-propan-2-ol; tetrahydrofuran / 0.33 h / 70 °C

With potassium tert-butylate; lithium diisopropyl amide; In tetrahydrofuran; tert-butyl alcohol;

DOI:10.1016/S0040-4020(01)00278-2

Reference yield:

3-(4-methoxyphenyl)-1-iodopropane (113379-13-8) → (2R,3R,RS)-(-)-2-[3-(4-methoxyphenyl)propyl]-2-(p-tolylsulfinyl)-1,3-diphenylaziridine (351388-30-2)

Guidance literature:

Multi-step reaction with 3 steps

1.1: lithium diisopropylamide / tetrahydrofuran / 0.17 h

1.2: 99 percent / tetrahydrofuran

2.1: lithium diisopropylamide / tetrahydrofuran / 0.17 h

2.2: 98 percent / tetrahydrofuran / 0.17 h

3.1: 79 percent / potassium tert-butoxide / 2-methyl-propan-2-ol; tetrahydrofuran / 0.33 h / 70 °C

With potassium tert-butylate; lithium diisopropyl amide; In tetrahydrofuran; tert-butyl alcohol;

DOI:10.1016/S0040-4020(01)00278-2

Reference yield:

1-chloro-4-(4-methoxyphenyl)-1-(p-tolylsulfinyl)butane → (2R,3R,RS)-(-)-2-[3-(4-methoxyphenyl)propyl]-2-(p-tolylsulfinyl)-1,3-diphenylaziridine (351388-30-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: lithium diisopropylamide / tetrahydrofuran / 0.17 h

1.2: 98 percent / tetrahydrofuran / 0.17 h

2.1: 79 percent / potassium tert-butoxide / 2-methyl-propan-2-ol; tetrahydrofuran / 0.33 h / 70 °C

With potassium tert-butylate; lithium diisopropyl amide; In tetrahydrofuran; tert-butyl alcohol;

DOI:10.1016/S0040-4020(01)00278-2

upstream raw materials:

(R)-chloromethyl p-tolyl sulfoxide

3-(4-methoxyphenyl)-1-iodopropane

Downstream raw materials:

(2S,3R)-(-)-2-decyl-2-[3-(4-methoxyphenyl)propyl]-1,3-diphenylaziridine

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