Technology Process of C15H18O2
There total 4 articles about C15H18O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
at 25 ℃;
for 16h;
DOI:10.1246/cl.2013.180
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dicyclohexyl-carbodiimide / acetonitrile / 6 h / 20 °C
2: O-tert-butyldiphenylsilyl (S)-β-homoserine lithium salt; water / dimethyl sulfoxide; dichloromethane / 24 h / 25 °C
3: trifluoroacetic acid / dichloromethane / 16 h / 25 °C
With
O-tert-butyldiphenylsilyl (S)-β-homoserine lithium salt; water; dicyclohexyl-carbodiimide; trifluoroacetic acid;
In
dichloromethane; dimethyl sulfoxide; acetonitrile;
2: |Michael Addition;
DOI:10.1246/cl.2013.180
- Guidance literature:
-
Multi-step reaction with 4 steps
1: water; sodium hydroxide / 20 °C
2: dicyclohexyl-carbodiimide / acetonitrile / 6 h / 20 °C
3: O-tert-butyldiphenylsilyl (S)-β-homoserine lithium salt; water / dimethyl sulfoxide; dichloromethane / 24 h / 25 °C
4: trifluoroacetic acid / dichloromethane / 16 h / 25 °C
With
O-tert-butyldiphenylsilyl (S)-β-homoserine lithium salt; water; dicyclohexyl-carbodiimide; trifluoroacetic acid; sodium hydroxide;
In
dichloromethane; dimethyl sulfoxide; acetonitrile;
3: |Michael Addition;
DOI:10.1246/cl.2013.180
![tert-butyl 3-oxo-2-[(R)-3-oxocycloheptyl]-3-phenylpropanoate](/Databaselist/images/loading.webp)
