cis,cis,trans-bis((pMe)thiolato)(carbonyl)2(triphenylphosphine)2ruthenium(II)*THF

Base Information

Chemical Name:cis,cis,trans-bis((pMe)thiolato)(carbonyl)2(triphenylphosphine)2ruthenium(II)*THF
CAS No.:136823-98-8
Molecular Formula:C₄H₈O*C₅₂H₄₄O₂P₂RuS₂
Molecular Weight:1000.18
Hs Code.:

Synonyms:cis,cis,trans-bis((pMe)thiolato)(carbonyl)2(triphenylphosphine)2ruthenium(II)*THF

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Chemical Property of cis,cis,trans-bis((pMe)thiolato)(carbonyl)2(triphenylphosphine)2ruthenium(II)*THF

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Technology Process of cis,cis,trans-bis((pMe)thiolato)(carbonyl)2(triphenylphosphine)2ruthenium(II)*THF

There total 6 articles about cis,cis,trans-bis((pMe)thiolato)(carbonyl)2(triphenylphosphine)2ruthenium(II)*THF which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 32240-58-7
cis,cis,trans-hydrido(Cl)(carbonyl)2(triphenylphosphine)2ruthenium(II)

: 10486-08-5
sodium p-thiocresolate

: 107031-82-3
cis,cis,trans-hydrido((pMeC₆H₄)thiolato)(carbonyl)2(triphenylphosphine)2ruthenium(II)

: 136823-98-8
cis,cis,trans-bis((pMe)thiolato)(carbonyl)2(triphenylphosphine)2ruthenium(II)*THF

Guidance literature:: In acetone; under Ar at 20°C overnight; vac. distn., (1)H and (31)P NMR detn.;

Reference yield: 85.0%

: 35880-54-7,61647-76-5,184490-77-5,65635-71-4
{ruthenium⁽⁰⁾ dicarbonyltris(triphenylphosphine)}

: 103-19-5
di(p-tolyl) disulfide

: 136823-98-8
cis,cis,trans-bis((pMe)thiolato)(carbonyl)2(triphenylphosphine)2ruthenium(II)*THF

Guidance literature:: In tetrahydrofuran; byproducts: PPh3; under N2 or Ar, react. in soln. at room temp. for 4.5 h in dark; concn. by vac. distn., addn. of hexane;