cis,cis,trans-hydrido(Cl)(carbonyl)2(triphenylphosphine)2ruthenium(II)

Base Information

Chemical Name:cis,cis,trans-hydrido(Cl)(carbonyl)2(triphenylphosphine)2ruthenium(II)
CAS No.:32240-58-7
Molecular Formula:C₃₈H₃₁ClO₂P₂Ru
Molecular Weight:718.133
Hs Code.:

Synonyms:cis,cis,trans-hydrido(Cl)(carbonyl)2(triphenylphosphine)2ruthenium(II)

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Chemical Property of cis,cis,trans-hydrido(Cl)(carbonyl)2(triphenylphosphine)2ruthenium(II)

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Technology Process of cis,cis,trans-hydrido(Cl)(carbonyl)2(triphenylphosphine)2ruthenium(II)

There total 15 articles about cis,cis,trans-hydrido(Cl)(carbonyl)2(triphenylphosphine)2ruthenium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: Ru(trans-styryl)(CO)2(PPh₃)2(Cp(CO)3Mo)*H₂O

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 56144-64-0,52555-05-2,32240-58-7
dicarbonylchlorohydridobis(triphenylphosphine)ruthenium(II)

Guidance literature:: With HCl; In benzene; byproducts: Mo(C5H5)Cl(CO)3; at room temp.; IR, NMR;
DOI:10.1246/cl.1992.69

Reference yield: 65.0%

: 60020-25-9,78216-70-3
aquadicarbonylhydridobis(triphenylphosphine)ruthenium(II) tetrafluoroborate

: 56144-64-0,52555-05-2,32240-58-7
dicarbonylchlorohydridobis(triphenylphosphine)ruthenium(II)

Guidance literature:: With LiCl; In methanol; N2-atmosphere; refluxing for few min; pptn. on cooling, collection, washing (MeOH, ether), drying (vac.); elem. anal.;
DOI:10.1039/DT9760000719

Reference yield: 40.0%

: 15529-49-4,41756-81-4
tris(triphenylphosphine)ruthenium(II) chloride

: 32240-58-7
cis,cis,trans-hydrido(Cl)(carbonyl)2(triphenylphosphine)2ruthenium(II)

Guidance literature:: With H₂; CO; In N,N-dimethyl acetamide; 30 min. in degassed soln. under 1 atm H2, replacing H2 with 1 atm of CO for 35 min; concn. of soln., addn. of MeOH, filtn. of ppt., drying in vac., (1)H, (31)P and (13)C NMR and IR detn.;