4-nitrophenyl benzyl[(2,4-dioxo-1,2,3,4-tetrahydropyrimidin-5-yl)methyl]carbamate

Base Information

Chemical Name:4-nitrophenyl benzyl[(2,4-dioxo-1,2,3,4-tetrahydropyrimidin-5-yl)methyl]carbamate
CAS No.:910045-01-1
Molecular Formula:C₁₉H₁₆N₄O₆
Molecular Weight:396.359
Hs Code.:

Synonyms:4-nitrophenyl benzyl[(2,4-dioxo-1,2,3,4-tetrahydropyrimidin-5-yl)methyl]carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-nitrophenyl benzyl[(2,4-dioxo-1,2,3,4-tetrahydropyrimidin-5-yl)methyl]carbamate

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Technology Process of 4-nitrophenyl benzyl[(2,4-dioxo-1,2,3,4-tetrahydropyrimidin-5-yl)methyl]carbamate

There total 2 articles about 4-nitrophenyl benzyl[(2,4-dioxo-1,2,3,4-tetrahydropyrimidin-5-yl)methyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 897387-50-7
5-(benzylaminomethyl)uracil

: 7693-46-1
4-Nitrophenyl chloroformate

: 910045-01-1
4-nitrophenyl benzyl[(2,4-dioxo-1,2,3,4-tetrahydropyrimidin-5-yl)methyl]carbamate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; for 20h;
DOI:10.1055/s-2006-941604

Reference yield:

: 100-46-9
benzylamine

: 910045-01-1
4-nitrophenyl benzyl[(2,4-dioxo-1,2,3,4-tetrahydropyrimidin-5-yl)methyl]carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / ethanol; H₂O / 20 h / Heating

2: 82 percent / Et₃N / tetrahydrofuran / 20 h / 20 °C

With triethylamine; In tetrahydrofuran; ethanol; water; 1: Mannich reaction;
DOI:10.1055/s-2006-941604