3-(3-chlorophenyl)glutaric anhydride

Base Information

Chemical Name:3-(3-chlorophenyl)glutaric anhydride
CAS No.:4759-62-0
Molecular Formula:C₁₁H₉ClO₃
Molecular Weight:224.644
Hs Code.:

Synonyms:3-(3-chlorophenyl)glutaric anhydride

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Chemical Property of 3-(3-chlorophenyl)glutaric anhydride

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Technology Process of 3-(3-chlorophenyl)glutaric anhydride

There total 4 articles about 3-(3-chlorophenyl)glutaric anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 587-04-2
m-Chlorobenzaldehyde

: 4759-62-0
3-(3-chlorophenyl)glutaric anhydride

Guidance literature:: Multi-step reaction with 3 steps

1.1: piperidine / ethanol / 20 h / 20 °C

2.1: sodium hydroxide / 2 h / Reflux

2.2: Cooling with ice

3.1: acetyl chloride / 2 h / Reflux

With piperidine; acetyl chloride; sodium hydroxide; In ethanol;
DOI:10.1021/jm2005892

Reference yield:

: 4759-58-4
acide (chloro-3 phenyl)-3 glutarique

: 4759-62-0
3-(3-chlorophenyl)glutaric anhydride

Guidance literature:: With acetyl chloride; for 2h; Reflux;
DOI:10.1021/jm2005892

Reference yield:

: 4759-55-1
2-<3-Chlor-phenyl>-4-hydroxy-4-methyl-6-oxo-cyclohexan-1,3-dicarbonsaeure-diethylester

: 4759-62-0
3-(3-chlorophenyl)glutaric anhydride

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / 2 h / Reflux

1.2: Cooling with ice

2.1: acetyl chloride / 2 h / Reflux

With acetyl chloride; sodium hydroxide;
DOI:10.1021/jm2005892